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| Naji, M. |
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| Motta, Antonella |
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| Aletan, Dirar |
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| Mohamed, Tarek |
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| Ertürk, Emre |
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| Taccardi, Nicola |
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| Kononenko, Denys |
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| Petrov, R. H. | Madrid |
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| Alshaaer, Mazen | Brussels |
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| Bih, L. |
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| Casati, R. |
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| Muller, Hermance |
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| Kočí, Jan | Prague |
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| Šuljagić, Marija |
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| Kalteremidou, Kalliopi-Artemi | Brussels |
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| Azam, Siraj |
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| Ospanova, Alyiya |
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| Blanpain, Bart |
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| Ali, M. A. |
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| Popa, V. |
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| Rančić, M. |
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| Ollier, Nadège |
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| Azevedo, Nuno Monteiro |
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| Landes, Michael |
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| Rignanese, Gian-Marco |
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Farjas, Jordi
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Topics
Publications (18/18 displayed)
- 2022Chemical and Microstructural Nanoscale Homogeneity in Superconducting YBa2Cu3O7-x Films Derived from Metal-Propionate Fluorine-free Solutionscitations
- 2021High Performance of Superconducting YBa2Cu3O7 Thick Films Prepared by Single-Deposition Inkjet Printing
- 2020Ultrafast transient liquid assisted growth of high current density superconducting films
- 2020Ultrafast transient liquid assisted growth of high current density superconducting films
- 2020Relevance of the Formation of Intermediate Non-Equilibrium Phases in YBa2Cu3O7-x Film Growth by Transient Liquid-Assisted Growth
- 2020Elucidation of the decomposition reactions of low-fluorine YBa2Cu3O7-x precursors during film pyrolysis
- 2019Thermal decomposition of CuProp2: In-situ analysis of film and powder pyrolysiscitations
- 2018Epitaxial superconducting GdBa2Cu3O7−δ /Gd2O3 nanocomposite thin films from advanced low-fluorine solutionscitations
- 2015Thermal analysis of metal organic precursors for functional oxide preparation: Thin films versus powderscitations
- 2015The effect of volatiles on the measurement of the reaction heat by differential scanning calorimetrycitations
- 2013Thermal decomposition of barium trifluoroacetate thin filmscitations
- 2013Thermoanalytical study of the decomposition of yttrium trifluoroacetate thin filmscitations
- 2012Synthesis of nanocrystalline ceria thin films by low-temperature thermal decomposition of Ce-propionatecitations
- 2011Thermoanalytical study of the formation mechanism of yttria from yttrium acetatecitations
- 2009Characterization of amorphous and nanostructured Si films by differential scanning calorimetrycitations
- 2007Numerical model of solid phase transformations governed by nucleation and growth: Microstructure development during isothermal crystallizationcitations
- 2002Calorimetry of hydrogen desorption from a-Si nanoparticlescitations
- 2001Enhancement of oxidation rate of a-Si nanoparticles during dehydrogenationcitations
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article
Thermal decomposition of CuProp2: In-situ analysis of film and powder pyrolysis
Abstract
The thermal decomposition of CuProp2 in the form of film and powder was studied in different atmospheres by means of thermal analysis techniques (TG-MS, TG-IR, EGA), chemical-structural methods (FTIR, XRD, EA) and computational thermochemistry (VASP/PBE). The decomposition mechanism in terms of volatiles evolved was disclosed with the aid of ab-initio modeling; it was found to be dependent on the gas diffusion in and out of the sample and accelerated by a humid atmosphere. In films, the copper redox behavior showed sensitivity to the residual atmosphere. Finally, the role of the metal center is discussed in the frame of a general decomposition mechanism for metal propionates.