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Naji, M. |
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Motta, Antonella |
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Aletan, Dirar |
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Mohamed, Tarek |
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Ertürk, Emre |
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Taccardi, Nicola |
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Kononenko, Denys |
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Petrov, R. H. | Madrid |
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Alshaaer, Mazen | Brussels |
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Bih, L. |
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Casati, R. |
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Muller, Hermance |
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Kočí, Jan | Prague |
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Šuljagić, Marija |
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Kalteremidou, Kalliopi-Artemi | Brussels |
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Azam, Siraj |
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Ospanova, Alyiya |
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Blanpain, Bart |
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Ali, M. A. |
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Popa, V. |
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Rančić, M. |
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Ollier, Nadège |
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Azevedo, Nuno Monteiro |
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Landes, Michael |
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Rignanese, Gian-Marco |
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Másilko, Jiří
Brno University of Technology
in Cooperation with on an Cooperation-Score of 37%
Topics
Publications (10/10 displayed)
- 2023Early and middle stages of multicomponent cement hydration under the effect of geothermal water and increased temperaturescitations
- 2022Effect of alkali salts on the hydration process of belite clinkercitations
- 2022The thermal analysis of zinc oxide‑contaminated Portland cement blended with thiocyanates and determination of their effect on hydration and propertiescitations
- 2022Synthesis, Structural, Morphological and Thermal Characterization of Five Different Silica-Polyethylene Glycol-Chlorogenic Acid Hybrid Materials ; Syntéza, strukturní, morfologická a tepelná charakterizace pěti různých hybridních materiálů silika-polyethylenglykol-kyselina chlorogenovácitations
- 2021The Effect of Crystallization and Phase Transformation on the Mechanical and Electrochemical Corrosion Properties of Ni-P Coatingscitations
- 2020The Characterization of Fixation of Ba, Pb, and Cu in Alkali-Activated Fly Ash/Blast Furnace Slag Matrixcitations
- 2020Synthesis conditions influencing formation of MAPbBr3 perovskite nanoparticles prepared by the ligandassisted precipitation methodcitations
- 2020Influence of Pb Dosage on Immobilization Characteristics of Different Types of Alkali-Activated Mixtures and Mortarscitations
- 2020The effect of heat-treatment on properties of Ni-P coatings deposited on AZ91 magnesium alloycitations
- 2020Cement Kiln By-Pass Dust: An Effective Alkaline Activator for Pozzolanic Materialscitations
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article
The Characterization of Fixation of Ba, Pb, and Cu in Alkali-Activated Fly Ash/Blast Furnace Slag Matrix
Abstract
The fixation of heavy metals (Ba, Cu, Pb) in an alkali-activated matrix was investigated. The matrix consisted of fly ash and blast furnace slag (BFS). The mixture of NaOH and Na-silicate was used as alkaline activator. Three analytical techniques were used to describe the fixation of heavy metals—X-ray photoelectron spectroscopy (XPS), scanning electron microscopy (SEM) equipped with energy dispersive X-ray spectroscopy (EDS), and X-ray powder diffraction (XRD). All heavy metals formed insoluble salts after alkaline activation. Ba was fixed as BaSO4, and only this product was crystalline. EDS mapping showed that Ba was cumulated in some regions and formed clusters. Pb was present in the form of Pb(OH)2 and was dispersed throughout the matrix on the edges of BFS grains. Cu was fixed as Cu(OH)2 and also was cumulated in some regions and formed clusters. Cu was present in two different chemical states; apart from Cu(OH)2, a Cu–O bond was also identified.