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Naji, M. |
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Motta, Antonella |
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Aletan, Dirar |
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Mohamed, Tarek |
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Ertürk, Emre |
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Taccardi, Nicola |
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Kononenko, Denys |
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Petrov, R. H. | Madrid |
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Alshaaer, Mazen | Brussels |
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Bih, L. |
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Casati, R. |
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Muller, Hermance |
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Kočí, Jan | Prague |
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Šuljagić, Marija |
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Kalteremidou, Kalliopi-Artemi | Brussels |
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Azam, Siraj |
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Ospanova, Alyiya |
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Blanpain, Bart |
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Ali, M. A. |
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Popa, V. |
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Rančić, M. |
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Ollier, Nadège |
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Azevedo, Nuno Monteiro |
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Landes, Michael |
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Rignanese, Gian-Marco |
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Másilko, Jiří
Brno University of Technology
in Cooperation with on an Cooperation-Score of 37%
Topics
Publications (10/10 displayed)
- 2023Early and middle stages of multicomponent cement hydration under the effect of geothermal water and increased temperaturescitations
- 2022Effect of alkali salts on the hydration process of belite clinkercitations
- 2022The thermal analysis of zinc oxide‑contaminated Portland cement blended with thiocyanates and determination of their effect on hydration and propertiescitations
- 2022Synthesis, Structural, Morphological and Thermal Characterization of Five Different Silica-Polyethylene Glycol-Chlorogenic Acid Hybrid Materials ; Syntéza, strukturní, morfologická a tepelná charakterizace pěti různých hybridních materiálů silika-polyethylenglykol-kyselina chlorogenovácitations
- 2021The Effect of Crystallization and Phase Transformation on the Mechanical and Electrochemical Corrosion Properties of Ni-P Coatingscitations
- 2020The Characterization of Fixation of Ba, Pb, and Cu in Alkali-Activated Fly Ash/Blast Furnace Slag Matrixcitations
- 2020Synthesis conditions influencing formation of MAPbBr3 perovskite nanoparticles prepared by the ligandassisted precipitation methodcitations
- 2020Influence of Pb Dosage on Immobilization Characteristics of Different Types of Alkali-Activated Mixtures and Mortarscitations
- 2020The effect of heat-treatment on properties of Ni-P coatings deposited on AZ91 magnesium alloycitations
- 2020Cement Kiln By-Pass Dust: An Effective Alkaline Activator for Pozzolanic Materialscitations
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article
The Effect of Crystallization and Phase Transformation on the Mechanical and Electrochemical Corrosion Properties of Ni-P Coatings
Abstract
This paper deals with the study of the crystallization and phase transformation of Ni-P coatings deposited on AZ91 magnesium alloy. Prepared samples were characterized in terms of surface morphology and elemental composition by means of scanning electron microscopy with energy-dispersive spectroscopy analysis. The results of X-ray diffraction analysis and differential scanning calorimetry suggested that increasing the phosphorus content caused Ni-P coatings to develop an amorphous character. The crystallization of Ni was observed at 150, 250, and 300 °C for low-, medium- and high-phosphorus coatings, respectively. The Ni crystallite size increased with increasing temperature and decreasing P content. Conversely, the presence of the Ni3P phase was observed at a maximum peak of 320 °C for the high-phosphorus coating, whereas the crystallization of the Ni3P phase shifted to higher temperatures with decreasing P content. The Ni3P crystallite size increased with increasing temperature and increasing P content. An increase in microhardness due to the arrangement of Ni atoms and Ni3P precipitation was observed. The deposition of as-deposited Ni-P coatings led to an improvement in the corrosion resistance of AZ91. However, the heat treatment of coatings resulted in a deterioration in corrosion properties due to the formation of microcracks.