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Naji, M. |
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Motta, Antonella |
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Aletan, Dirar |
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Mohamed, Tarek |
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Ertürk, Emre |
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Taccardi, Nicola |
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Kononenko, Denys |
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Petrov, R. H. | Madrid |
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Alshaaer, Mazen | Brussels |
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Bih, L. |
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Casati, R. |
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Muller, Hermance |
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Kočí, Jan | Prague |
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Šuljagić, Marija |
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Kalteremidou, Kalliopi-Artemi | Brussels |
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Azam, Siraj |
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Ospanova, Alyiya |
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Blanpain, Bart |
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Ali, M. A. |
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Popa, V. |
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Rančić, M. |
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Ollier, Nadège |
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Azevedo, Nuno Monteiro |
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Landes, Michael |
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Rignanese, Gian-Marco |
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Kaiser, Jozef
Epoka University
in Cooperation with on an Cooperation-Score of 37%
Topics
Publications (15/15 displayed)
- 2023Fatigue behaviour of titanium scaffolds with hierarchical porosity produced by material extrusion additive manufacturingcitations
- 2023Interlaboratory comparison for quantitative chlorine analysis in cement pastes with laser induced breakdown spectroscopycitations
- 2023Interlaboratory comparison for quantitative chlorine analysis in cement pastes with laser induced breakdown spectroscopycitations
- 2022Degradable magnesium-hydroxyapatite interpenetrating phase composites processed by current assisted metal infiltration in additive-manufactured porous preformscitations
- 2022Contour laser strategy and its benefits for lattice structure manufacturing by selective laser melting technologycitations
- 2021Interface Behavior and Interface Tensile Strength of a Hardened Concrete Mixture with a Coarse Aggregate for Additive Manufacturingcitations
- 2020Strength and fracture mechanism of iron reinforced tricalcium phosphate cermet fabricated by spark plasma sintering ; Pevnost a lomové mechanismy železem zpevněhého trikalcium fosfátového cermetu vyrobeného metodou spark plasma sinteringcitations
- 2020Influence of Scanning Strategies on Processing of Aluminum Alloy EN AW 2618 Using Selective Laser Meltingcitations
- 2020Heat treatment induced phase transformations in zirconia and yttriastabilized zirconia monolithic aerogelscitations
- 2020High strength, biodegradable and cytocompatible alpha tricalcium phosphate-iron composites for temporal reduction of bone fractures ; Vysoce pevné, biologicky odbouratelné a cytocompatibilní kompozity alfa trikalcium fosfát-železo pro časovou redukci fraktur kostícitations
- 2019Laboratory X-ray tomography for metal additive manufacturingcitations
- 2019SLM process parameters development of Cu-alloy Cu7.2Ni1.8Si1Crcitations
- 2018Accelerated hardening of nanotextured 3D-plotted self-setting calcium phosphate inkscitations
- 2017Fracture Mechanism of Interpenetrating Iron-Tricalcium Phosphate Composite ; Lomové mechanismy inpenetrovaného kompozizu železo - trikalcium fosfátcitations
- 2014Temperature effect on the microstructural development of Al–Ni layered binary couples produced by an unconventional methodcitations
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article
Heat treatment induced phase transformations in zirconia and yttriastabilized zirconia monolithic aerogels
Abstract
Monolithic, structurally stable zirconia (ZrO2) aerogels can be used in high temperature applications and as medical implants. The macroscopic properties of these solids can be fine-tuned by the appropriate thermal treatment of the amorphous aerogels. Herein, we investigate the thermally induced phase transitions of ZrO2 and yttria-stabilized zirconia (YSZ) monolithic aerogels. All aerogels were produced by an acid-catalyzed sol-gel technique and subsequent supercritical drying (SCD). A complete reaction mechanism is proposed for the formation of the wet gel network. Also, the phase transformations taking place during calcination were followed as function of temperature by in-situ X-ray diffraction measurements. Composition and size of the forming crystallites were calculated from the XRD data. Phase transition is controlled by the temperature-dependent growth of crystallite size during calcination up to 1200 °C. Both tetragonal and monoclinic zirconia form in pure ZrO2 aerogels, and a single tetragonal phase forms in YSZ aerogels. ; 2021-02-27