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Naji, M. |
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Motta, Antonella |
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Aletan, Dirar |
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Mohamed, Tarek |
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Ertürk, Emre |
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Taccardi, Nicola |
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Kononenko, Denys |
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Petrov, R. H. | Madrid |
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Alshaaer, Mazen | Brussels |
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Bih, L. |
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Casati, R. |
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Muller, Hermance |
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Kočí, Jan | Prague |
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Šuljagić, Marija |
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Kalteremidou, Kalliopi-Artemi | Brussels |
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Azam, Siraj |
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Ospanova, Alyiya |
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Blanpain, Bart |
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Ali, M. A. |
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Popa, V. |
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Rančić, M. |
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Ollier, Nadège |
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Azevedo, Nuno Monteiro |
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Landes, Michael |
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Rignanese, Gian-Marco |
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Stojanović, Jovica
in Cooperation with on an Cooperation-Score of 37%
Topics
Publications (12/12 displayed)
- 2024Exploring the Efficiency of Magnetic Separation and Gravity Concentration for Valorizing Pb-Zn Smelter Slag in a Circular Economy Frameworkcitations
- 2024The effect of sintering temperature on cavitation erosion in glass–ceramics based on coal fly ashcitations
- 2024Reapplication Potential of Historic Pb–Zn Slag with Regard to Zero Waste Principlescitations
- 2024Modification of selectively acid-etched halloysite by mucoadhesive chitosan derivatives: new bionanocomposites with improved functional propertiescitations
- 2023Crystallization characteristics of bioactive polyphosphate glasses
- 2023Single-step, electrophoretically deposited hydroxyapatite/poly(vinyl alcohol)/chitosan/gentamicin coating for biomedical applicationscitations
- 2023Application of pyrophyllite in high-temperature treated building materialscitations
- 2023Hydroxyapatite/poly(vinyl alcohol)/chitosan coating with gentamicin for orthopedic implantscitations
- 2022Possibility of “Topionica” - Veles Pb-Zn slag valorization by gravity concentration procedure
- 2020Microstructure and Phase Composition Of Steatite Ceramics Sintered by Traditional and Spark Plasma Sinteringcitations
- 2019Synthesis and characterization of composites based on expanded vermiculite and ferrite spinels
- 2018Compound spinel as a masking pigment obtained by mechanochemical treatment
Places of action
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article
Microstructure and Phase Composition Of Steatite Ceramics Sintered by Traditional and Spark Plasma Sintering
Abstract
The influence of the sintering method on the mineral phase transformations and development of the crystalline microstructure of steatite ceramics was investigated. The steatite samples were fabricated from talc and bentonite as low-cost raw materials. Feldspar and barium carbonate, as fluxing agents, were altered in the steatite composition. Dilatometric analysis was applied in the monitoring of the dimensional changes and thereby densification of steatite during the traditional sintering (TS) procedure up to 1200 °C. Spark plasma sintering (SPS) method was used under the following sintering conditions: 100 °C/min heating rate, uniaxial pressure of 50 MPa; sintering temperature 800 °C/1 min or 1000 °C/2 min. Crystallinity changes and mineral phase transition during sintering were observed by X-ray diffraction technique. Microstructural visualization of the samples and the spatial arrangements of individual chemical elements were achieved via scanning electron microscopy equipped with the EDS mapping. It was found that SPS sintering facilitated all microstructural changes during high temperature treatment and shifted them to lower temperatures. SPS treatment conducted at 1000 °C resulted in maximum densification of the steatite powder compacts and the formation stabilized protoenstatite structure