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Forsyth, M.
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Publications (8/8 displayed)
- 2017Properties of High Na-Ion Content N-Propyl-N-Methylpyrrolidinium Bis(Fluorosulfonyl)Imide -Ethylene Carbonate Electrolytescitations
- 2016Inorganic-organic ionic liquid electrolytes enabling high energy-density metal electrodes for energy storagecitations
- 2016Recent developments in environment-friendly corrosion inhibitors for mild steel
- 2012Electrochemical etching of aluminium alloy in ionic liquids
- 2011Anodising AA5083 aluminium alloy using ionic liquids
- 2011Anodic oxidation of AZ31 Mg alloy in ionic liquid
- 2003Cerium acetylacetonates—new aspects, including the lamellar clathrate [Ce(acac)4]·10H2Ocitations
- 2001The synthesis of high molecular weight polybutene-1 catalyzed by Cp*Ti(OBz)3/MAO
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document
Electrochemical etching of aluminium alloy in ionic liquids
Abstract
<p>AA5083 aluminium alloy has been shown to be partially passivated by a 2-step anodic pre-treatment in Trihexyl(tetradecyl)phosphonium bis(trifluoromethylsulfonyl)amide ([P<sub>6,6,6,14</sub>][NTf<sub>2</sub>]) ionic liquid. Surface characterisation revealed that an electrochemical etching process had occurred, comparable to acid etching of aluminium. Scanning electron microscopy/energy dispersive x-ray spectroscopy results have established that magnesium dealloyed from the Mg<sub>2</sub>Si intermetallic particles and metal fluorides were deposited onto the remaining Mg<sub>2</sub>Si sites, which subsequently led to decreased anodic corrosion kinetics (to one third of the control) as well as an increase in the corrosion and pitting potentials. This unique electrochemical etching process offers a simple and quick method to improve the corrosion resistance of an aluminium alloy as it leads to a more uniform surface, in terms of defect size and distribution, compared to conventional acid etching. This process has the potential to be used as a pre-treatment to inhibit corrosion of AA5083 alloy.</p>