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Naji, M. |
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Motta, Antonella |
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Aletan, Dirar |
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Mohamed, Tarek |
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Ertürk, Emre |
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Taccardi, Nicola |
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Kononenko, Denys |
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Petrov, R. H. | Madrid |
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Alshaaer, Mazen | Brussels |
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Bih, L. |
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Casati, R. |
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Muller, Hermance |
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Kočí, Jan | Prague |
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Šuljagić, Marija |
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Kalteremidou, Kalliopi-Artemi | Brussels |
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Azam, Siraj |
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Ospanova, Alyiya |
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Blanpain, Bart |
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Ali, M. A. |
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Popa, V. |
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Rančić, M. |
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Ollier, Nadège |
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Azevedo, Nuno Monteiro |
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Landes, Michael |
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Rignanese, Gian-Marco |
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Horsewell, Andy
in Cooperation with on an Cooperation-Score of 37%
Topics
Publications (14/14 displayed)
- 2014A TEM Study on the Ti-Alloyed Grey Iron
- 2012Mechanical properties of low-density polyethylene filled by graphite nanoplateletscitations
- 2012A TEM Study on the Microstructure of Fine Flaky Graphite
- 2011Advanced 2D and 3D Electron Microscopy Analysis of Clay/PP Nanocomposites
- 20093-D Analysis of Graphite Nodules in Ductile Cast Iron Using FIB-SEM
- 2009Development of Focused Ion Beam technique for high speed steel 3D-SEM artefact fabrication
- 2008Changes in the tribological behavior of an epoxy resin by incorporating CuO nanoparticles and PTFE microparticlescitations
- 2008Ge nanoclusters in PECVD-deposited glass caused only by heat treatmentcitations
- 2007Grey-scale conversion X-ray mapping by EDS of multielement and multiphase layered microstructurescitations
- 2007Learning about materials science and technology by deconstructing modern products
- 2007Ge nanoclusters in PECVD-deposited glass after heat treating and electron irradiationcitations
- 2005Investigation on the traceability of three dimensional scanning electron microscope measurements based on the stereo-pair technique
- 2005Investigation on the traceability of three dimensional scanning electron microscope measurements based on the stereo-pair technique
- 2001Crack Growth along Interfaces in Porous Ceramic Layerscitations
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article
Investigation on the traceability of three dimensional scanning electron microscope measurements based on the stereo-pair technique
Abstract
An investigation was carried out concerning the traceability of dimensional measurements performed with the scanning electron microscope (SEM) using reconstruction of surface topography through stereo-photogrammetry. A theoretical description of the effects that the main instrumental variables and measurement parameters have on the reconstruction accuracy of any point on the surface of the object being imaged was undertaken. This description was based on the model function introduced by Piazzesi adapted for eucentrically tilted stereo-pairs. An analysis of the sensitivity coefficients for the vertical elevation model has identified the most important instrumental variables and measurement parameters to be the tilt angle and the magnification calibration. An equation describing the theoretically determined uncertainty of the vertical elevation was produced.An experimental investigation was carried out involving:(i) magnification calibration using a steel scale with 50 ìm pitch at low magnifications, and a 2D calibration grating with 2.120 ìm pitch at high magnifications;(ii) tilt angle calibration by laser interferometry;(iii) vertical elevation calibration using gauge-block steps;(iv) calibration in the vertical plane using two ISO 5436 type C roughness standards.Results from magnification calibration and tilt angle measurement were used for calculating the theoretical uncertainty on the vertical elevation. Experimental deviations measured on gauge-block steps showed slightly bigger values than those calculated from the theoretical model. Lateral measurement on the reconstructed three-dimensional topography of the type C roughness standards showed good agreement with the nominal profile wavelength values.An investigation was carried out concerning the traceability of dimensional measurements performed with the scanning electron microscope (SEM) using reconstruction of surface topography through stereo-photogrammetry. A theoretical description of the effects that the main instrumental variables and measurement parameters have on the reconstruction accuracy of any point on the surface of the object being imaged was undertaken. This description was based on the model function introduced by Piazzesi adapted for eucentrically tilted stereo-pairs. An analysis of the sensitivity coefficients for the vertical elevation model has identified the most important instrumental variables and measurement parameters to be the tilt angle and the magnification calibration. An equation describing the theoretically determined uncertainty of the vertical elevation was produced.An experimental investigation was carried out involving:(i) magnification calibration using a steel scale with 50 ìm pitch at low magnifications, and a 2D calibration grating with 2.120 ìm pitch at high magnifications;(ii) tilt angle calibration by laser interferometry;(iii) vertical elevation calibration using gauge-block steps;(iv) calibration in the vertical plane using two ISO 5436 type C roughness standards.Results from magnification calibration and tilt angle measurement were used for calculating the theoretical uncertainty on the vertical elevation. Experimental deviations measured on gauge-block steps showed slightly bigger values than those calculated from the theoretical model. Lateral measurement on the reconstructed three-dimensional topography of the type C roughness standards showed good agreement with the nominal profile wavelength values.An investigation was carried out concerning the traceability of dimensional measurements performed with the scanning electron microscope (SEM) using reconstruction of surface topography through stereo-photogrammetry. A theoretical description of the effects that the main instrumental variables and measurement parameters have on the reconstruction accuracy of any point on the surface of the object being imaged was undertaken. This description was based on the model function introduced by Piazzesi adapted for eucentrically tilted stereo-pairs. An analysis of the sensitivity coefficients for the vertical elevation model has identified the most important instrumental variables and measurement parameters to be the tilt angle and the magnification calibration. An equation describing the theoretically determined uncertainty of the vertical elevation was produced.An experimental investigation was carried out involving:(i) magnification calibration using a steel scale with 50 ìm pitch at low magnifications, and a 2D calibration grating with 2.120 ìm pitch at high magnifications;(ii) tilt angle calibration by laser interferometry;(iii) vertical elevation calibration using gauge-block steps;(iv) calibration in the vertical plane using two ISO 5436 type C roughness standards.Results from magnification calibration and tilt angle measurement were used for calculating the theoretical uncertainty on the vertical elevation. Experimental deviations measured on gauge-block steps sh...