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Naji, M. |
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Motta, Antonella |
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Aletan, Dirar |
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Mohamed, Tarek |
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Ertürk, Emre |
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Taccardi, Nicola |
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Kononenko, Denys |
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Petrov, R. H. | Madrid |
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Alshaaer, Mazen | Brussels |
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Bih, L. |
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Casati, R. |
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Muller, Hermance |
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Kočí, Jan | Prague |
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Šuljagić, Marija |
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Kalteremidou, Kalliopi-Artemi | Brussels |
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Azam, Siraj |
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Ospanova, Alyiya |
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Blanpain, Bart |
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Ali, M. A. |
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Popa, V. |
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Rančić, M. |
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Ollier, Nadège |
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Azevedo, Nuno Monteiro |
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Landes, Michael |
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Rignanese, Gian-Marco |
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Todt, Juraj
in Cooperation with on an Cooperation-Score of 37%
Topics
Publications (24/24 displayed)
- 2024Peculiarity of hydrogen absorption in duplex steels: Phase-selective lattice swelling and stress evolutioncitations
- 2023Deflecting Dendrites by Introducing Compressive Stress in Li7La3Zr2O12 Using Ion Implantationcitations
- 2023Metal–Matrix Composites from High‐Pressure Torsion with Functionalized Material Behavior
- 2023Influence of Hatch Strategy on Crystallographic Texture Evolution, Mechanical Anisotropy of Laser Beam Powder Bed Fused S316L Steelcitations
- 2023Design of high-strength martensitic steels by novel mixed-metal nanoprecipitates for high toughness and suppressed hydrogen embrittlementcitations
- 2023Deflecting Dendrites by Introducing Compressive Stress in Li7La3Zr2O12 Using Ion Implantation ; ENEngelskEnglishDeflecting Dendrites by Introducing Compressive Stress in Li7La3Zr2O12 Using Ion Implantationcitations
- 2023Ti$_{40}$Zr$_{10}$Cu$_{36}$Pd$_{14}$ bulk metallic glass as oral implant materialcitations
- 2023Manufacturing size effect on the structural and mechanical properties of additively manufactured Ti-6Al-4V microbeamscitations
- 2023Ti40Zr10Cu36Pd14 bulk metallic glass as oral implant materialcitations
- 2022Graded Inconel-stainless steel multi-material structure by inter- and intralayer variation of metal alloyscitations
- 2022Graded Inconel-stainless steel multi-material structure by inter- and intralayer variation of metal alloyscitations
- 2022Combining hardness measurements of a heat-treated crankshaft bearing with cross-sectional residual stress and retained austenite distributions measured by HEXRDcitations
- 2021Ion irradiation-induced localized stress relaxation in W thin film revealed by cross-sectional X-ray nanodiffractioncitations
- 2020Nanoscale stress distributions and microstructural changes at scratch track cross-sections of a deformed brittle-ductile CrN-Cr bilayercitations
- 2020Evolution of stress fields during crack growth and arrest in a brittle-ductile CrN-Cr clamped-cantilever analysed by X-ray nanodiffraction and modellingcitations
- 2019Anisotropy of fracture toughness in nanostructured ceramics controlled by grain boundary designcitations
- 2019Cross-sectional gradients of residual stresses, microstructure and phases in a nitrided steel revealed by 20 µm synchrotron X-ray diffraction
- 2018Influence of Annealing on Microstructure and Mechanical Properties of a Nanocrystalline CrCoNi Medium-Entropy Alloycitations
- 201830 nm X-ray focusing correlates oscillatory stress, texture and structural defect gradients across multilayered TiN-SiOx thin filmcitations
- 2018An investigation on shear banding and crystallographic texture of Ag–Cu alloys deformed by high-pressure torsioncitations
- 2017Phase Decomposition of a Single-Phase AlTiVNb High-Entropy Alloy after Severe Plastic Deformation and Annealingcitations
- 2016In-situ Observation of Cross-Sectional Microstructural Changes and Stress Distributions in Fracturing TiN Thin Film during Nanoindentationcitations
- 2016Integrated experimental and computational approach for residual stress investigation near through-silicon viascitations
- 2014Mono-textured nanocrystalline thin films with pronounced stress-gradientscitations
Places of action
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article
Cross-sectional gradients of residual stresses, microstructure and phases in a nitrided steel revealed by 20 µm synchrotron X-ray diffraction
Abstract
Cross-sectional gradients of residual stresses, phases, microstructure, composition and mechanical properties within the near-surface<br/>regions of thermo-chemical treated steels are decisive for the balanced mechanical properties of the final products. In this work, a<br/>correlative cross-sectional micro-analytics is introduced to assess those gradients in an exemplary nitrided steel sample to a depth<br/>of ~0.8 mm. Cross-sectional synchrotron X-ray microdiffraction with an energy of 87.1 keV and a spatial resolution of 20 µm was<br/>performed in transmission diffraction geometry. At first, a methodology to evaluate residual stress magnitudes from two-dimensional<br/>X-ray diffraction data is discussed. The data from a ~2.5 mm long sample gauge volume indicate complex residual stresses and<br/>near-surface microstructure gradients with a maximal compressive stress of ~-400 MPa, descending diffraction peak broadening and<br/>variable crystallographic texture. The results correlate well with the complementary analyses of Vickers micro hardness and sample<br/>cross-sectional morphology. In summary, the correlative cross-sectional micro-analytics documents the possibility to determine and<br/>correlate a variety of mechanical, structural, morphological and chemical sample parameters obtained using cutting-edge characterization approaches. The complex experimental data can be further used to adjust and verify numerical and technological models.