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Naji, M. |
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Motta, Antonella |
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Aletan, Dirar |
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Mohamed, Tarek |
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Ertürk, Emre |
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Taccardi, Nicola |
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Kononenko, Denys |
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Petrov, R. H. | Madrid |
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Alshaaer, Mazen | Brussels |
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Bih, L. |
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Casati, R. |
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Muller, Hermance |
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Kočí, Jan | Prague |
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Šuljagić, Marija |
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Kalteremidou, Kalliopi-Artemi | Brussels |
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Azam, Siraj |
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Ospanova, Alyiya |
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Blanpain, Bart |
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Ali, M. A. |
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Popa, V. |
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Rančić, M. |
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Ollier, Nadège |
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Azevedo, Nuno Monteiro |
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Landes, Michael |
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Rignanese, Gian-Marco |
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Scott, Thomas Bligh
in Cooperation with on an Cooperation-Score of 37%
Topics
Publications (23/23 displayed)
- 2023An investigation of the reaction of metallic uranium with oxygen/nitrogen gas mixturescitations
- 2022Investigating the mechanical behaviour of Fukushima MCCI using synchrotron Xray tomography and digital volume correlationcitations
- 2021Investigating the microstructure and mechanical behaviour of simulant "lava-like" fuel containing materials from the Chernobyl reactor unit 4 meltdowncitations
- 2018A study of dynamic nanoscale corrosion initiation events by HS-AFMcitations
- 2018In-situ, time resolved monitoring of uranium in BFS:OPC grout. Part 2citations
- 2017Investigating corrosion using high-speed AFM
- 2017In-situ, time resolved monitoring of uranium in BFS:OPC grout. Part 1:citations
- 2016The crystallographic structure of the air-grown oxide on depleted uranium metalcitations
- 2016Structural effects in UO 2 thin films irradiated with U ionscitations
- 2016Atomic-scale Studies of Uranium Oxidation and Corrosion by Water Vapourcitations
- 2016Structural effects in UO2 thin films irradiated with U ionscitations
- 2015Nuclear waste viewed in a new lightcitations
- 2015Structural deformation of metallic uranium surrounding hydride growth sitescitations
- 2015Characterisation of electrodeposited polycrystalline uranium dioxide thin films on nickel foil for industrial applicationscitations
- 2015An investigation into heterogeneity in a single vein-type uranium ore depositcitations
- 2015The effects of metal surface geometry on the formation of uranium hydridecitations
- 2015The role of ferrite in Type 316H austenitic stainless steels on the susceptibility to creep cavitationcitations
- 2015An investigation on the persistence of uranium hydride during storage of simulant nuclear waste packagescitations
- 2014Electronic properties of γ-U and superconductivity of U–Mo alloyscitations
- 2013A surface science study of the initial stages of hydrogen corrosion on uranium metal and the role played by grain microstructurecitations
- 2013Altering the hydriding behaviour of uranium metal by induced oxide penetration around carbo-nitride inclusionscitations
- 2011Enhanced reactivity of nanoscale iron particles through a vacuum annealing process.citations
- 2010Oxidative corrosion of carbide inclusions at the surface of uranium metal during exposure to water vapour.
Places of action
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conferencepaper
Investigating corrosion using high-speed AFM
Abstract
The unpredictable nature of stress corrosion cracking (SCC) calls for further research into the mechanisms under which it and other forms of destructive corrosion occur. Observation of crack initiation at the nanoscale could give valuable insight into the processes that take place within metals during SCC. The high-speed atomic force microscope (HS-AFM) we have developed operates at speeds orders of magnitude faster than conventional atomic force microscopes (AFMs), and is capable of capturing multiple frames per second, allowing for dynamic events to be observed directly in real-time, with nanometre lateral resolution and subatomic height resolution [1]. Furthermore, HS-AFM is a valuable tool for studying solid-liquid interfaces and as such has the potential for in situ corrosion studies [1]. The applications for HS-AFMs are still relatively unexplored, and advances in HS-AFM technology are ongoing. In this paper, corrosion mechanisms were investigated using our contact mode HS-AFM. Hardness induced topographic maps of the surface of sensitised austenitic stainless steels have been produced, in which chromium carbide precipitation can be clearly seen by means of proper surface preparation [2]. Furthermore, a micro strain rig was custom built such that samples could be imaged under stress, alongside corrosive conditions, for investigations into SCC initiation. Laferrere et al. have previously demonstrated the use of HS-AFM to image nanoscale corrosion events, with parallel electrochemical control [3]. The research presented here builds upon this previous investigation, further substantiating the capability and potential of HS-AFM for applications in materials and corrosion science.