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Naji, M. |
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Motta, Antonella |
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Aletan, Dirar |
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Mohamed, Tarek |
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Ertürk, Emre |
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Taccardi, Nicola |
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Kononenko, Denys |
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Petrov, R. H. | Madrid |
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Alshaaer, Mazen | Brussels |
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Bih, L. |
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Casati, R. |
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Muller, Hermance |
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Kočí, Jan | Prague |
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Šuljagić, Marija |
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Kalteremidou, Kalliopi-Artemi | Brussels |
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Azam, Siraj |
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Ospanova, Alyiya |
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Blanpain, Bart |
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Ali, M. A. |
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Popa, V. |
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Rančić, M. |
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Ollier, Nadège |
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Azevedo, Nuno Monteiro |
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Landes, Michael |
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Rignanese, Gian-Marco |
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Beigbeder, Alexandre
in Cooperation with on an Cooperation-Score of 37%
Topics
Publications (12/12 displayed)
- 2024Impact of flax fibre micro-structural features on composite damage observed through micro-CT characterisationcitations
- 2023Tracking the changes into mechanical properties and ultrastructure of flax cell walls during a dynamic heating treatment
- 2023Tracking the changes into mechanical properties and ultrastructure of flax cell walls during a dynamic heating treatment
- 2023In-situ monitoring of changes in ultrastructure and mechanical properties of flax cell walls during controlled heat treatmentcitations
- 2023In-Situ Monitoring Of The Ultrastructure And Mechanical Properties Of Flax Cell Walls During Controlled Heat Treatment
- 2023In-Situ Monitoring Of The Ultrastructure And Mechanical Properties Of Flax Cell Walls During Controlled Heat Treatment
- 2016Influence of constituents and process parameters on mechanical properties of flax fibre-reinforced polyamide 11 compositecitations
- 2010Marine fouling release silicone/carbon nanotube nanocomposite coatings: On the importance of the nanotube dispersion statecitations
- 2009On The Effect of Carbon Nanotubes on The Wettability and Surface Morphology of Hydrosilylation-Curing Silicone Coatings
- 2008CH-p interactions as the driving force for silicone-based nanocomposites with exceptional rheological and thermal propertiescitations
- 2008Poly(dimethylsiloxane)/carbon nanotubes nanocomposites: (nano)structured coatings for the control of marine biofouling
- 2008CH-π interactions as the driving force for silicone-based nanocomposites with exceptional propertiescitations
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document
In-Situ Monitoring Of The Ultrastructure And Mechanical Properties Of Flax Cell Walls During Controlled Heat Treatment
Abstract
Plant fibres are increasingly used as reinforcements, especially in thermoplastic composites. Understanding the impact of temperature on the properties of these fibres is an important issue for the manufacturing of high-performance materials with minimal defects. In this work, the structural evolution and mechanical behaviour of flax fibre cell walls were dynamically monitored by temperature-controlled X-ray diffraction and nanoindentation from 25 to 230°C; detailed biochemical analysis was also conducted on fibre samples after each heating step. With increasing temperature up to 230°C, a drop in the local mechanical performance of the flax cell walls was measured. This was associated with a decrease in the packing of the cellulose crystal lattice (increase in d-spacing d200), as well as significant mass losses measured by TGA and changes in the biochemical composition, i.e. non-cellulosic polysaccharides (NCPs) of the middle lamellae but also of the cell walls. This work, which proposes for the first time an in-situ investigation of the dynamic temperature evolution of the flax cell wall properties, evidences the reversible behaviour of their crystalline structure (i.e. cellulose) and local mechanical properties after cooling to room temperature, even after exposure to high temperatures.