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Zhang, Jizhen
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article
Laboratory based X-ray Microscopy
Abstract
Here we report on a new laboratory based X-ray facility for X-ray microscopy and dynamic materials testing. Based on a dual port, high brightness Excillum Metal Jet X-ray source, beamline I offers fully automated SAXS-WAXS capabilities while beamline II is modular to enable rapid switching from polychromatic diffraction to micro-computer tomography (MicroCT). The attributes of the new facility are highlighted by 3 case studies.The first case study demonstrates correlation microscopy at different length scales- microCT is used assess macro-scale porosity in Ti3C2Tx MXene, while SAXS-WAXS is used to interrogate channel alignment and porosity at the nm level. Case study 2 addresses the role of boron nitride sheets as a grain size refinement approach for additive manufacturing of Ti alloys.Finally, in-situ observation of plasticity onset in lightweight Mg alloys is presented.