| People | Locations | Statistics |
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| Naji, M. |
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| Motta, Antonella |
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| Aletan, Dirar |
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| Mohamed, Tarek |
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| Ertürk, Emre |
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| Taccardi, Nicola |
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| Kononenko, Denys |
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| Petrov, R. H. | Madrid |
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| Alshaaer, Mazen | Brussels |
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| Bih, L. |
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| Casati, R. |
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| Muller, Hermance |
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| Kočí, Jan | Prague |
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| Šuljagić, Marija |
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| Kalteremidou, Kalliopi-Artemi | Brussels |
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| Azam, Siraj |
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| Ospanova, Alyiya |
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| Blanpain, Bart |
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| Ali, M. A. |
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| Popa, V. |
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| Rančić, M. |
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| Ollier, Nadège |
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| Azevedo, Nuno Monteiro |
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| Landes, Michael |
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| Rignanese, Gian-Marco |
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Tack, Pieter
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Publications (7/7 displayed)
- 2023Hafnium oxide nanocrystals for contrast enhanced vascular casting : from mechanistic insight to application
- 2022The influence of bases on thermal decomposition synthesis of LaF3
- 2020An X-ray ray tracing simulation code for mono- and polycapillaries : description, advances and applicationcitations
- 2020Highly sensitive nondestructive rare earth element detection by means of wavelength-dispersive X-ray fluorescence spectroscopy enabled by an energy dispersive pn-charge-coupled-device detectorcitations
- 2017Sensing the framework state and guest molecules in MIL-53(Al) via the electron paramagnetic resonance spectrum of V-IV dopant ionscitations
- 2016Confocal depth-resolved micro-X-ray absorption spectroscopy study of chemically strengthened boroaluminosilicate glassescitations
- 2016Enhanced gas sorption and breathing properties of the new sulfone functionalized COMOC-2 metal organic frameworkcitations
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conferencepaper
The influence of bases on thermal decomposition synthesis of LaF3
Abstract
Nanothermometry is a fast-developing field of research due to the need of remote, precise, reliable and non-invasive temperature sensing in real time. This is both important for research, aswell as for industrial applications. However, new nanomaterials suitable for nanothermometry are often difficult to design as the synthesis might be challenging to control, and the fine-tuning of morphology, crystallinity and size is a sophisticated task. Schlenk line based synthesis are a well-known and frequently used route to grow nanoparticles for nanothermometry. However, reports on LaF3 synthesized employing a Schlenk line based thermal decomposition route are very rare.In this presentation we will overview our work carried out on the preparation of nanosized and well-dispersed LaF3 and the influence of different bases, namely LiOH, KOH, NaOH and NaF, used in a thermal decomposition Schlenk line synthesis.It has been reported before that an increase in the respective base and with it the pH value was assumed to accelerate the release of CF3COO- ions.1 Chien et.al linked this to an accelerated growth of LaF3 nanocrystals. Using varied reaction conditions we have worked to optimize the best synthesis route for the development of the nano-sized LaF3.