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Espeau, Philippe
Unité de Technologies Chimiques et Biologiques pour la Santé
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Publications (5/5 displayed)
- 2017Determination of the glass transition temperature of difficult samples by Flash DSC
- 2016Crystal structure determination and thermal behavior upon melting of p-synephrinecitations
- 2013Crystallographic and Pressure-Temperature State Diagram Approach for the Phase Behavior and Polymorphism Study of Glutaric Acidcitations
- 2011Physicochemical Stability of Solid Dispersions of Enantiomeric or Racemic Ibuprofen in Stearic Acidcitations
- 2011Solid-State Characterization of Enantiomeric and Racemic Hydrated and Anhydrous Zinc-Pidolate Complexescitations
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document
Determination of the glass transition temperature of difficult samples by Flash DSC
Abstract
Crystalline pharmaceutical substances often decompose immediately before or during melting. To determine the glass transition temperature, the substance must be melted and then cooled as rapidly as possible so that decomposition and crystallization do not occur. In many cases, the heating and cooling rates of conventional DSCs are not high enough for this purpose. The METTLER TOLEDO Flash DSC however offers new possibilities. This is illustrated in this article using prednisolone as an example.