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Schick, Christoph
University of Rostock
in Cooperation with on an Cooperation-Score of 37%
Topics
Publications (15/15 displayed)
- 2022Bulk enthalpy of melting of Poly (l-lactic acid) (PLLA) determined by fast scanning chip calorimetry
- 2021Crystal Nucleation and Growth in Cross-Linked Poly(ε-caprolactone) (PCL)citations
- 2021Nucleation behaviour and microstructure of single Al-Si12 powder particles rapidly solidified in a fast scanning calorimetercitations
- 2020Stability of crystal nuclei of poly (butylene isophthalate) formed near the glass transition temperature
- 2019Differential fast scanning calorimetry as analytical tool for mimicking melting and solidification in additive manufacturing
- 2019The Effect of Backbone Rigidity on the Glass Transition of Polymers of Intrinsic Microporosity Probed by Fast Scanning Calorimetrycitations
- 2019Enthalpy relaxation of polyamide 11 of different morphology far below the glass transition temperature
- 2019Review of the quench sensitivity of aluminium alloys: analysis of the kinetics and nature of quench-induced precipitationcitations
- 2018Cold-crystallization of poly(butylene 2,6-naphthalate) following Ostwald's rule of stagescitations
- 2017Determination of the glass transition temperature of difficult samples by Flash DSC
- 2015Control of precipitation during heat treatments based on DSC experiments
- 2015Temperature dependency of nucleation efficiency of carbon nanotubes in PET and PBTcitations
- 2014Crystallization of poly(ε-caprolactone)/MWCNT composites: a combined SAXS/WAXS, electrical and thermal conductivity studycitations
- 2014Kinetics of nucleation and crystallization in poly(butylene succinate) nanocompositescitations
- 2013Competitive crystallization of a propylene/ethylene random copolymer filled with a β-nucleating agent and multi-walled carbon nanotubes. conventional and ultrafast DSC studycitations
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document
Determination of the glass transition temperature of difficult samples by Flash DSC
Abstract
Crystalline pharmaceutical substances often decompose immediately before or during melting. To determine the glass transition temperature, the substance must be melted and then cooled as rapidly as possible so that decomposition and crystallization do not occur. In many cases, the heating and cooling rates of conventional DSCs are not high enough for this purpose. The METTLER TOLEDO Flash DSC however offers new possibilities. This is illustrated in this article using prednisolone as an example.