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Naji, M. |
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Motta, Antonella |
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Aletan, Dirar |
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Mohamed, Tarek |
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Ertürk, Emre |
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Taccardi, Nicola |
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Kononenko, Denys |
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Petrov, R. H. | Madrid |
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Alshaaer, Mazen | Brussels |
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Bih, L. |
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Casati, R. |
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Muller, Hermance |
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Kočí, Jan | Prague |
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Šuljagić, Marija |
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Kalteremidou, Kalliopi-Artemi | Brussels |
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Azam, Siraj |
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Ospanova, Alyiya |
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Blanpain, Bart |
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Ali, M. A. |
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Popa, V. |
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Rančić, M. |
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Ollier, Nadège |
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Azevedo, Nuno Monteiro |
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Landes, Michael |
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Rignanese, Gian-Marco |
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Simmons, Mark
University of Birmingham
in Cooperation with on an Cooperation-Score of 37%
Topics
Publications (17/17 displayed)
- 2024Design of slurries for 3D printing of sodium-ion battery electrodescitations
- 2023Comparison between RANS and 3D-PTV measurements of Newtonian and non-Newtonian fluid flows in a stirred vessel in the transitional regimecitations
- 2023Thermomechanical Responses of Microcracks in a Honeycomb Particulate Filter
- 2022Rheology and structure of lithium‐ion battery electrode slurriescitations
- 2021Understanding the effects of processing conditions on the formation of lamellar gel networks using a rheological approachcitations
- 2021Lagrangian investigations of a stirred tank fluid flow using 3D-PTVcitations
- 2020Ironmaking and Steelmaking Slags As Sustainable Adsorbents For Industrial Effluents And Wastewater Treatmentcitations
- 2017Investigating the impact of operating conditions on the extent of additive mixing during thermoplastic polymer extrusioncitations
- 2016Agglomeration in counter-current spray drying towers. Part A: Particle growth and the effect of nozzle heightcitations
- 2016A comparison of methods for in-situ discrimination of imaged phase boundaries using Electrical Capacitance Tomography
- 2016The impact of process parameters on the purity and chemical properties of lignin extracted from miscanthus x giganteus using a modified organosolv method
- 2013An Assessment of the Influence of Gas Turbine Lubricant Thermal Oxidation Test Method Parameters Towards the Development of a New Engine Representative Laboratory Test Methodcitations
- 2013Kinetics of metals adsorption in acid mine drainage treatment with blast furnace slag
- 2009Influence of surfactant upon air entrainment hysteresis in curtain coatingcitations
- 2007Influence of vicosity and impingement speed on intense hydrodynamic assist in curtain coatingcitations
- 2006Hysteresis and non-uniqueness in the speed of onset of instability in curtain coatingcitations
- 2006Influence of the flow field in curtain coating onto a prewet substratecitations
Places of action
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booksection
The impact of process parameters on the purity and chemical properties of lignin extracted from miscanthus x giganteus using a modified organosolv method
Abstract
<p>This work evaluates the purity and chemical properties of lignin extracted directly from Miscanthus x giganteus using a modified organosolv method (direct extraction) with lignin obtained from Miscanthus x giganteus which had been subjected to sequential sub-critical water mediated hydrolysis of increasing severity (sequential extraction). The data obtained were subjected to statistical analysis to ensure significant difference (p < 0.05) unless stated otherwise. The percentage of biomass solubilisation from sequential extraction was 45.5% and greater than the value of 35.6% obtained by direct extraction. The percentage of delignification from sequential and direct extraction was 58.0% and 81.5%, respectively. An assessment of percentage of lignin recovery after precipitation from direct extraction was 69.3% whereas the sequential extraction yielded 70.3%; the results were not significantly different (p=0.38) suggesting there was no negative impact of repeatedly processing biomass prior to lignin recovery using the same experimental conditions. The purity of the precipitated lignin and lignin derived from dried supernatant by sequential extraction was 91.5% and 23.7%, respectively, of higher purity than from direct extraction (88.4% and 14.1%, respectively). The chemical properties of precipitated lignin were further characterised by Fourier Transform Infrared Spectroscopy (FTIR). This showed that the Miscanthus x giganteus which is subjected to sequential extraction yielded high purity lignin than from direct extraction. Overall, the conceptual design of this work to sequentially process biomass is a promising method for recovery of multiple naturally occurring building blocks including hemicellulose, cellulose and lignin, which then become the feedstock for various applications.</p>