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Polychroniadis, G.
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article
Electron microscopy study of (Fe-Co)-Nb-Si-B alloys
Abstract
<p>Phases produced during crystallization of (Fe<sub>1</sub>Co <sub>4</sub>)<sub>73</sub>Nb<sub>7</sub>Si<sub>5</sub>B<sub>15</sub> amorphous alloy were studied by means of conventional and in-situ heating transmission electron microscopy. Differences in structure, morphology and grain size distributions are discussed. Apparent discrepancies in crystallization kinetics in thinned - originally amorphous, in-situ annealed samples versus samples a-priori annealed and thinned are shown to originate from sample dimensions and preparation methods. Information thus obtained is used for indication of the importance of surface and bulk effects during phase transformations. Results are correlated with the classical analysis of transformations from amorphous state.</p>