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- 2023Hydrogen bonding patterns and C—H...π interactions in the structure of the antiparkinsonian drug (<i>R</i>)-rasagiline mesylate determined using laboratory and synchrotron X-ray powder diffraction datacitations
- 2022Crystal structure from X-ray powder diffraction data, DFT-D calculation, Hirshfeld surface analysis, and energy frameworks of (<i>RS</i>)-trichlormethiazidecitations
- 2020Preparación del compuesto Beta/MCM-41: un material con una isoterma de adsorción-desorción poco convencional
- 2018Caracterización estructural mediante difracción de rayos X de polvo de la zeolita Beta: un análisis por el método Le Bail
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Preparación del compuesto Beta/MCM-41: un material con una isoterma de adsorción-desorción poco convencional
Abstract
The preparation of a micro/mesoporous Beta/MCM-41 material by recrystallization of Beta zeolite in an alkaline medium is reported. The material is characterized by X-Ray Powder Diffraction (XRPD), Fourier Transformed Infrared spectroscopy (FT-IR), Scanning Electron Microscopy (SEM) and nitrogen physisorption. XRPD results corroborate the presence of the Beta zeolite and the MCM-41 material. Nitrogen adsorption-desorption isotherm showed a non-conventional behavior suggesting the presence of a structured and hierarchical system in which the micro- and mesoporous phase coexist.