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Naji, M. |
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Motta, Antonella |
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Aletan, Dirar |
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Mohamed, Tarek |
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Ertürk, Emre |
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Taccardi, Nicola |
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Kononenko, Denys |
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Petrov, R. H. | Madrid |
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Alshaaer, Mazen | Brussels |
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Bih, L. |
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Casati, R. |
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Muller, Hermance |
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Kočí, Jan | Prague |
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Šuljagić, Marija |
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Kalteremidou, Kalliopi-Artemi | Brussels |
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Azam, Siraj |
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Ospanova, Alyiya |
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Blanpain, Bart |
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Ali, M. A. |
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Popa, V. |
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Rančić, M. |
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Ollier, Nadège |
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Azevedo, Nuno Monteiro |
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Landes, Michael |
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Rignanese, Gian-Marco |
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Tahira, Aneela
in Cooperation with on an Cooperation-Score of 37%
Topics
Publications (13/13 displayed)
- 2023An advanced PdNPs@MoS<sub>2</sub> nanocomposite for efficient oxygen evolution reaction in alkaline mediacitations
- 2023Transforming NiCo2O4 nanorods into nanoparticles using citrus lemon juice enhancing electrochemical properties for asymmetric supercapacitor and water oxidationcitations
- 2023Green-Mediated Synthesis of NiCo2O4 Nanostructures Using Radish White Peel Extract for the Sensitive and Selective Enzyme-Free Detection of Uric Acidcitations
- 2023Transforming NiCo 2 O 4 nanorods into nanoparticles using citrus lemon juice enhancing electrochemical properties for asymmetric supercapacitor and water oxidationcitations
- 2023Grapefruit juice containing rich hydroxyl and oxygenated groups capable of transforming 1D structure of NiCo 2 O 4 into 0D with excessive surface vacancies for promising energy conversion and storage applicationscitations
- 2022Co₂FeO₄@rGO composite: Towards trifunctional water splitting in alkaline mediacitations
- 2022NiCo2O4 nanostructures loaded onto pencil graphite rod: An advanced composite material for oxygen evolution reactioncitations
- 2022A green approach for the preparation of ZnO@C nanocomposite using agave americana plant extract with enhanced photodegradationcitations
- 2022Enhanced Electrocatalytic Properties of Co3O4 Nanocrystals Derived from Hydrolyzed Polyethyleneimines in Water/Ethanol Solvents for Electrochemical Detection of Cholesterolcitations
- 2021Synthesis of composite material of cobalt oxide (Co3O4) with hydroxide functionalized multi-walled carbon nanotubes (MWCNTs) for electrochemical determination of uric acid
- 2019An efficient bifunctional electrocatalyst based on a nickel iron layered double hydroxide functionalized Co3O4 core shell structure in alkaline mediacitations
- 2019Advanced Co3O4-CuO nano-composite based electrocatalyst for efficient hydrogen evolution reaction in alkaline mediacitations
- 2019An advanced and efficient Co3O4/C nanocomposite for the oxygen evolution reaction in alkaline mediacitations
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document
Synthesis of composite material of cobalt oxide (Co3O4) with hydroxide functionalized multi-walled carbon nanotubes (MWCNTs) for electrochemical determination of uric acid
Abstract
The gout is mainly found due to accumulation of uric acid crystals into the joints which produces the inflammatory symptoms. Thus, it is highly demanded to detect uric acid from our body. Herein, we prepare a composite material of cobalt oxide (Co3O4) with hydroxide functionalized multi-walled carbon nanotubes (MWCNTs) by hydrothermal method. The composite material is used for the modification of glassy carbon electrode (GCE) and investigated for the electrochemical determination of uric acid (UA). The analytical techniques such as scanning electron microscopy (SEM), powder X-ray diffraction (XRD), energy dispersive spectroscopy (EDS) and Fourier Infra-red spectroscopy (FTIR) are used to characterize the composite material. The Co3O4 exhibits a dendrite morphology and very well chemically coupled with MWCNTs. The elemental analysis confirms the presence of cobalt (Co), oxygen (O) and carbon (C) as main constituent of the composite material. The Co3O4 exhibitsa cubic unit cell crystallography in the composite system. The FTIR study reveals the characteristic bands of Co–O bands in the composite material. The cyclic voltammetry isused to study the electrochemical properties of prepared materials. The composite sample with highest percentage of MWCNTs shows an excellent electrochemical activity towards the oxidation of uric acid in phosphate buffer solution pH 7.3. The enzyme free uric acid sensor possesses a linear range of 0.1 mM to 3 mM with a quantified limit of detection of 0.005 ± 0.0023 mM. The modified electrode is stable, selective, and very sensitive towards uric acid, therefore it may be used for the monitoring of uric acid from clinical samples. The proposed composite material can be of great interest for energy and biomedical fields.