Materials Map

Discover the materials research landscape. Find experts, partners, networks.

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The Materials Map is an open tool for improving networking and interdisciplinary exchange within materials research. It enables cross-database search for cooperation and network partners and discovering of the research landscape.

The dashboard provides detailed information about the selected scientist, e.g. publications. The dashboard can be filtered and shows the relationship to co-authors in different diagrams. In addition, a link is provided to find contact information.

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The Materials Map is still under development. In its current state, it is only based on one single data source and, thus, incomplete and contains duplicates. We are working on incorporating new open data sources like ORCID to improve the quality and the timeliness of our data. We will update Materials Map as soon as possible and kindly ask for your patience.

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in Cooperation with on an Cooperation-Score of 37%

Topics

Publications (1/1 displayed)

  • 2024Efficient nanoscale imaging of solid-state phase transitions by transmission electron microscopy demonstrated on vanadium dioxide nanoparticlescitations

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Horák, Michal
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Kabát, Jiří
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Konečná, Andrea
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Kepič, Peter
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Ligmajer, Filip
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Šikola, Tomáš
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Křápek, Vlastimil
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2024

Co-Authors (by relevance)

  • Horák, Michal
  • Kabát, Jiří
  • Konečná, Andrea
  • Kepič, Peter
  • Ligmajer, Filip
  • Šikola, Tomáš
  • Křápek, Vlastimil
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document

Efficient nanoscale imaging of solid-state phase transitions by transmission electron microscopy demonstrated on vanadium dioxide nanoparticles

  • Horák, Michal
  • Kabát, Jiří
  • Konečná, Andrea
  • Kepič, Peter
  • Hájek, Martin
  • Ligmajer, Filip
  • Šikola, Tomáš
  • Křápek, Vlastimil
Abstract

We present annular dark field scanning transmission electron microscopy (ADF-STEM) as an efficient, fast, and non-destructive nanoscale tool for monitoring solid-state phase transition. Using metal-insulator transition in vanadium dioxide nanoparticles as an example, we characterize lattice and electronic signatures of the phase transition using analytical transmission electron microscopy including diffraction and electron energy-loss spectroscopy. We demonstrate that ADF-STEM shows a clear contrast across the transition, interpreted with the help of convergent electron beam diffraction as stemming from the crystal-lattice modification accompanying the transition. In addition, ADF-STEM utilizes 3--6 orders of magnitude lower electron dose when compared to electron microscopy techniques able to reveal the phase transition with the same spatial resolution and universality. The benefits of ADF-STEM are emphasized by recording a full hysteresis loop for the metal-insulator transition of a single vanadium dioxide nanoparticle. Our study opens the prospect for fast, non-destructive, large-area and nanoscale characterization of solid-state phase transitions.

Topics
  • nanoparticle
  • phase
  • phase transition
  • transmission electron microscopy
  • vanadium
  • spectroscopy