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| Naji, M. |
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| Mohamed, Tarek |
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| Azevedo, Nuno Monteiro |
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Mohamadou, Aminou
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Publications (4/4 displayed)
- 2020Synthesis and crystal structure of a zinc(II) coordination polymer: N-(2-pyridylmethyl)- L-alanine)isothiocyanate Zn(II)citations
- 2020Synthesis and crystal structure of a zinc(II) coordination polymer: N-(2-pyridylmethyl)- L-alanine)isothiocyanate Zn(II)citations
- 2016Electrodeposition of Ni, Fe and Ni-Fe Alloys in Two Ionic Liquids: (tri (n-butyl) [2-methoxy-2-oxoethyl] Ammonium bis (trifluoromethylsulfonyl) [BuGBOEt] [Tf2N] and (1-butyl-1- methylpyrrolidinium bis trifluoromethylsulfonyl) imide ([P1,4] [Tf2N])citations
- 2007Equilibrium and structural studies of copper and nickel complexes with a pentadentate ligand providing amide, amine and pyridyl nitrogen donors. Crystal structure of the dinuclear nickel(II) complexcitations
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article
Synthesis and crystal structure of a zinc(II) coordination polymer: N-(2-pyridylmethyl)- L-alanine)isothiocyanate Zn(II)
Abstract
<jats:p>The title compound, N-(2-pyridylmethyl)-L-alanine) zinc(II), [Zn(C10H11N3O2S)], a coordination polymer derived from the mixed ligands, N-(2-pyridylmethyl)-L-alanine (HL1) and ammonium thiocyanide (L2) has been synthesized and characterized by IR spectroscopy, 1H-NMR, elemental analysis, thermogravimetric analysis and single crystal x-ray structure determination.The single crystal X-ray structure analysis of the title compoundreveals a molecular polymeric compound that crystallizes in the orthorhombic crystal system and P2(1)2(1)2(1) space group. The ligand acts as a bridge between adjacent zinc(II) centres, each of which adopts a five-coordinate geometry. Zinc bonds to two N atoms and one O atom of HL1, one N atom of L2 and one O atom of another HL1 ligand. This is confirmed by IR spectroscopy. Thermogravimetric analysis shows a one-step decomposition of the complex to leave a zinc sulfide residue.
 
 KEY WORDS: Zinc(II), N-(2-pyridylmethyl)-(L)-alanine) ligand, Isothiocyanate, Coordination polymer, Single crystal structure
 
 Bull. Chem. Soc. Ethiop. 2020, 34(2), 285-293
 DOI: https://dx.doi.org/10.4314/bcse.v34i2.7</jats:p>