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Naji, M. |
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Motta, Antonella |
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Aletan, Dirar |
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Mohamed, Tarek |
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Ertürk, Emre |
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Taccardi, Nicola |
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Kononenko, Denys |
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Petrov, R. H. | Madrid |
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Alshaaer, Mazen | Brussels |
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Bih, L. |
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Casati, R. |
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Muller, Hermance |
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Kočí, Jan | Prague |
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Šuljagić, Marija |
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Kalteremidou, Kalliopi-Artemi | Brussels |
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Azam, Siraj |
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Ospanova, Alyiya |
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Blanpain, Bart |
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Ali, M. A. |
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Popa, V. |
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Rančić, M. |
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Ollier, Nadège |
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Azevedo, Nuno Monteiro |
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Landes, Michael |
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Rignanese, Gian-Marco |
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Schmidt, Jochen
in Cooperation with on an Cooperation-Score of 37%
Topics
Publications (11/11 displayed)
- 2022Control of Crystallization of PBT-PC Blends by Anisotropic SiO2 and GeO2 Glass Flakescitations
- 2022Dry powder coating in additive manufacturingcitations
- 2022Biodegradable Polylactide Supraparticle Powders with Functional Additives for Biomedical Additive Manufacturingcitations
- 2022Abrasion-Induced Acceleration of Melt Crystallisation of Wet Comminuted Polybutylene Terephthalate (PBT)citations
- 2021Synthesis and characterization of manganese containing mesoporous bioactive glass nanoparticles for biomedical applications
- 2021Particle Lagrangian CFD Simulation and Experimental Characterization of the Rounding of Polymer Particles in a Downer Reactor with Direct Heatingcitations
- 2021A novel, precipitated polybutylene terephthalate feedstock material for powder bed fusion of polymers (PBF): Material development and initial PBF processabilitycitations
- 2020Cu, Zn doped borate bioactive glasses: antibacterial efficacy and dose-dependent in vitro modulation of murine dendritic cellscitations
- 2020Development of Polyoxymethylene Particles via the Solution-Dissolution Process and Application to the Powder Bed Fusion of Polymerscitations
- 2018Synthesis and characterization of manganese containing mesoporous bioactive glass nanoparticles for biomedical applicationscitations
- 2015Local densification of a single micron sized silica sphere by uniaxial compressioncitations
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article
Abrasion-Induced Acceleration of Melt Crystallisation of Wet Comminuted Polybutylene Terephthalate (PBT)
Abstract
Within this contribution, the effect of grinding media wear on the melt crystallisation of polybutylene terephthalate (PBT) is addressed. PBT was wet ground in a stirred media mill in ethanol using different grinding media beads (silica, chrome steel, cerium-stabilised and yttrium-stabilised zirconia) at comparable stress energies with the intention to use the obtained particles as feed materials for the production of feedstocks for laser powder bed fusion additive manufacturing (PBF-AM). In PBF-AM, the feedstock’s optical, rheological and especially thermal properties—including melt crystallisation kinetics—strongly influence the processability and properties of the manufactured parts. The influence of process parameters and used grinding media during wet comminution on the optical properties, crystal structure, molar mass distribution, inorganic content (wear) and thermal properties of the obtained powders is discussed. A grinding media-dependent acceleration of the melt crystallisation could be attributed to wear particles serving as nuclei for heterogeneous crystallisation. Yttrium-stabilised zirconia grinding beads proved to be the most suitable for the production of polymer powders for the PBF process in terms of (fast) comminution kinetics, unchanged optical properties and the least accelerated crystallisation kinetics.