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Naji, M. |
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Motta, Antonella |
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Aletan, Dirar |
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Mohamed, Tarek |
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Ertürk, Emre |
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Taccardi, Nicola |
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Kononenko, Denys |
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Petrov, R. H. | Madrid |
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Alshaaer, Mazen | Brussels |
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Bih, L. |
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Casati, R. |
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Muller, Hermance |
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Kočí, Jan | Prague |
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Šuljagić, Marija |
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Kalteremidou, Kalliopi-Artemi | Brussels |
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Azam, Siraj |
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Ospanova, Alyiya |
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Blanpain, Bart |
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Ali, M. A. |
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Popa, V. |
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Rančić, M. |
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Ollier, Nadège |
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Azevedo, Nuno Monteiro |
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Landes, Michael |
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Rignanese, Gian-Marco |
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Zabihi, Omid
in Cooperation with on an Cooperation-Score of 37%
Topics
Publications (7/7 displayed)
- 2021Metal–organic framework structure–property relationships for high-performance multifunctional polymer nanocomposite applicationscitations
- 2019Low-Cost Carbon Fibre Derived from Sustainable Coal Tar Pitch and Polyacrylonitrile: Fabrication and Characterisationcitations
- 20192D transition metal dichalcogenide nanomaterials: advances, opportunities, and challenges in multi-functional polymer nanocompositescitations
- 2019A Hydrothermal-Assisted Ball Milling Approach for Scalable Production of High-Quality Functionalized MoS2 Nanosheets for Polymer Nanocompositescitations
- 2015Enhanced thermal stability and lifetime of epoxy nanocomposites using covalently functionalized clay: experimental and modellingcitations
- 2015One-pot synthesis of aminated multi-walled carbon nanotube using thiol-ene click chemistry for improvement of epoxy nanocomposites propertiescitations
- 2013Study on a novel thermoset nanocomposite form DGEBA–cycloaliphatic diamine and metal nanoparticlescitations
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article
A Hydrothermal-Assisted Ball Milling Approach for Scalable Production of High-Quality Functionalized MoS2 Nanosheets for Polymer Nanocomposites
Abstract
<jats:p>The most known analogue of graphene, molybdenum disulfide (MoS2) nanosheet, has recently captured great interest because it can present properties beyond graphene in several high technological applications. Nonetheless, the lack of a feasible, sustainable, and scalable approach, in which synthesizing and functionalization of 2H-MoS2 nanosheets occur simultaneously, is still a challenge. Herein, a hydrothermal treatment has been utilised to reduce the effect of breaking mechanisms on the lateral size of produced nanosheets during the ball milling process. It was demonstrated that the hydrothermal pre-treatment led to the initial intercalation of an organic molecule such as 4,4’-diaminodiphenyl sulfone (DDS) within the stacked MoS2 sheets. Such a phenomenon can promote the horizontal shear forces and cause sliding and peeling mechanisms to be the dominated ones during low energy ball milling. Such combined methods can result in the production of 2H functionalized MoS2 nanosheets. The resultant few layers showed an average lateral dimension of more than 640 nm with the thickness as low as 6 nm and a surface area as high as 121.8 m2/g. These features of the synthesised MoS2 nanosheets, alongside their functional groups, can result in fully harnessing the reinforcing potential of MoS2 nanosheets for improvement of mechanical properties in different types of polymeric matrices.</jats:p>