Materials Map

Discover the materials research landscape. Find experts, partners, networks.

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The Materials Map is an open tool for improving networking and interdisciplinary exchange within materials research. It enables cross-database search for cooperation and network partners and discovering of the research landscape.

The dashboard provides detailed information about the selected scientist, e.g. publications. The dashboard can be filtered and shows the relationship to co-authors in different diagrams. In addition, a link is provided to find contact information.

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The Materials Map is still under development. In its current state, it is only based on one single data source and, thus, incomplete and contains duplicates. We are working on incorporating new open data sources like ORCID to improve the quality and the timeliness of our data. We will update Materials Map as soon as possible and kindly ask for your patience.

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Fulem, Michal

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University of Chemistry and Technology

in Cooperation with on an Cooperation-Score of 37%

Topics

Publications (6/6 displayed)

  • 2023Heat Capacities of N-Acetyl Amides of Glycine, L-Alanine, L-Valine, L-Isoleucine, and L-Leucine1citations
  • 2023Solid–Liquid Equilibrium in Co-Amorphous Systems: Experiment and Prediction5citations
  • 2020A combined thermodynamic and crystallographic study of 1,3-diisopropylnaphthalene3citations
  • 2020Impact of Hot-Melt Extrusion Processing Conditions on Physicochemical Properties of Amorphous Solid Dispersions Containing Thermally Labile Acrylic Copolymer18citations
  • 2020Glucose-modified carbosilane dendrimers: Interaction with model membranes and human serum albumin9citations
  • 2020Heat Capacities of l -Alanine, l -Valine, l -Isoleucine, and l -Leucine: Experimental and Computational Study31citations

Places of action

Chart of shared publication
Růžička, Květoslav
5 / 7 shared
Havlín, Jakub
2 / 3 shared
Štejfa, Vojtěch
3 / 6 shared
Pokorný, Václav Hoffmann
1 / 1 shared
Lieberzeitová, Eliška
1 / 1 shared
Zemánková, Alžběta
1 / 1 shared
Hassouna, Fatima
2 / 7 shared
Klajmon, Martin
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Rohlíček, Jan
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Mahnel, Tomáš
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Skořepová, Eliška
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Eigner, Václav
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Schroder, Bernd
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Mathers, Alex
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Malinová, Lenka
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Merna, Jan
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Bryszewska, Maria
1 / 22 shared
Malý, Jan
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Müllerová, Monika
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Wrobel, Dominika
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Kubíková, Radka
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Klajnert-Maculewicz, Barbara
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Strašák, Tomáš
1 / 4 shared
Červinka, Ctirad
1 / 5 shared
Pokorný, Václav
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Chart of publication period
2023
2020

Co-Authors (by relevance)

  • Růžička, Květoslav
  • Havlín, Jakub
  • Štejfa, Vojtěch
  • Pokorný, Václav Hoffmann
  • Lieberzeitová, Eliška
  • Zemánková, Alžběta
  • Hassouna, Fatima
  • Klajmon, Martin
  • Rohlíček, Jan
  • Mahnel, Tomáš
  • Skořepová, Eliška
  • Eigner, Václav
  • Schroder, Bernd
  • Mathers, Alex
  • Malinová, Lenka
  • Merna, Jan
  • Bryszewska, Maria
  • Malý, Jan
  • Müllerová, Monika
  • Wrobel, Dominika
  • Kubíková, Radka
  • Klajnert-Maculewicz, Barbara
  • Strašák, Tomáš
  • Červinka, Ctirad
  • Pokorný, Václav
OrganizationsLocationPeople

article

Heat Capacities of N-Acetyl Amides of Glycine, L-Alanine, L-Valine, L-Isoleucine, and L-Leucine

  • Fulem, Michal
  • Růžička, Květoslav
  • Havlín, Jakub
  • Štejfa, Vojtěch
  • Pokorný, Václav Hoffmann
  • Lieberzeitová, Eliška
Abstract

As a follow-up to our effort to establish reliable thermodynamic data for amino acids, the heat capacity and phase behavior are reported for N-acetyl glycine amide (CAS RN: 2620-63-5), N-acetyl-L-alanine amide (CAS RN: 15962-47-7), N-acetyl-L-valine amide (CAS RN: 37933-88-3), N-acetyl-L-isoleucine amide (CAS RN: 56711-06-9), and N-acetyl-L-leucine amide (CAS RN: 28529-34-2). Prior to heat capacity measurement, thermogravimetric analysis and X-ray powder diffraction were performed to determine decomposition temperatures and initial crystal structures, respectively. The crystal heat capacities of the five N-acetyl amino acid amides were measured by Tian–Calvet calorimetry in the temperature interval (266–350 K), by power compensation DSC in the temperature interval (216–471 K), and by relaxation (heat-pulse) calorimetry in the temperature interval (2–268 K). As a result, reference heat capacities and thermodynamic functions for the crystalline phase from 0 K up to 470 K were developed. © 2023 by the authors.

Topics
  • crystalline phase
  • thermogravimetry
  • differential scanning calorimetry
  • decomposition
  • heat capacity