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Naji, M. |
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Motta, Antonella |
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Aletan, Dirar |
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Mohamed, Tarek |
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Ertürk, Emre |
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Taccardi, Nicola |
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Kononenko, Denys |
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Petrov, R. H. | Madrid |
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Alshaaer, Mazen | Brussels |
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Bih, L. |
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Casati, R. |
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Muller, Hermance |
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Kočí, Jan | Prague |
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Šuljagić, Marija |
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Kalteremidou, Kalliopi-Artemi | Brussels |
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Azam, Siraj |
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Ospanova, Alyiya |
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Blanpain, Bart |
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Ali, M. A. |
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Popa, V. |
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Rančić, M. |
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Ollier, Nadège |
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Azevedo, Nuno Monteiro |
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Landes, Michael |
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Rignanese, Gian-Marco |
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Schafler, Erhard
in Cooperation with on an Cooperation-Score of 37%
Topics
Publications (15/15 displayed)
- 2024Verifying the cytotoxicity of a biodegradable zinc alloy with nanodiamond sensorscitations
- 2024Radial dependence of thermal, structural and micro deformation characteristics in Cu-Zr-Al bulk metallic glass subjected to high pressure torsioncitations
- 2024Effect of V content on the microstructure and mechanical properties of HPT nanostructured CoCrFeMnNiV x high entropy alloys
- 2023Comprehensive thermal analysis of a high stability Cu–Zr–Al bulk metallic glass subjected to high-pressure torsioncitations
- 2023From unlikely pairings to functional nanocomposites: FeTi–Cu as a model systemcitations
- 2022Structure-dynamics relationships in cryogenically deformed bulk metallic glasscitations
- 2022Thermal, Microstructural and Electrochemical Hydriding Performance of a Mg65Ni20Cu5Y10 Metallic Glass Catalyzed by CNT and Processed by High-Pressure Torsioncitations
- 2021In Situ Synchrotron X‐Ray Diffraction during High‐Pressure Torsion Deformation of Ni and NiTicitations
- 2021Properties of HPT-Processed Large Bulks of p-Type Skutterudite DD0.7Fe3CoSb12 with ZT > 1.3citations
- 2021Enhancing the Mechanical Properties of Biodegradable Mg Alloys Processed by Warm HPT and Thermal Treatmentscitations
- 2021High-Velocity Stretching of Renewable Polymer Blendscitations
- 2020The effects of severe plastic deformation and/or thermal treatment on the mechanical properties of biodegradable mg-alloyscitations
- 2020Advanced Immersion Testing of Model Mg-Alloys for Biomedical Applicationscitations
- 2020Anomalous Evolution of Strength and Microstructure of High-Entropy Alloy CoCrFeNiMn after High-Pressure Torsion at 300 and 77 Kcitations
- 2017Dislocation Movement Induced by Molecular Relaxations in Isotactic Polypropylenecitations
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article
The effects of severe plastic deformation and/or thermal treatment on the mechanical properties of biodegradable mg-alloys
Abstract
In this study, five MgZnCa alloys with low alloy content and high biocorrosion resistance were investigated during thermomechanical processing. As documented by microhardness and tensile tests, high pressure torsion (HPT)-processing and subsequent heat treatments led to strength increases of up to 250%; as much as about 1/3 of this increase was due to the heat treatment. Microstructural analyses by electron microscopy revealed a significant density of precipitates, but estimates of the Orowan strength exhibited values much smaller than the strength increases observed. Calculations using Kirchner’s model of vacancy hardening, however, showed that vacancy concentrations of 10−⁵ could have accounted for the extensive hardening observed, at least when they formed vacancy agglomerates with sizes around 50‒100 nm. While such an effect has been suggested for a selected Mg-alloy already in a previous paper of the authors, in this study the effect was substantiated by combined quantitative evaluations from differential scanning calorimetry and X-ray line profile analysis. Those exhibited vacancy concentrations of up to about 10−3 with a marked percentage being part of vacancy agglomerates, which has been confirmed by evaluations of defect specific activation migration enthalpies. The variations of Young’s modulus during HPT-processing and during the subsequent thermal treatments were small. Additionally, the corrosion rate did not markedly change compared to that of the homogenized state.