Materials Map

Discover the materials research landscape. Find experts, partners, networks.

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The Materials Map is an open tool for improving networking and interdisciplinary exchange within materials research. It enables cross-database search for cooperation and network partners and discovering of the research landscape.

The dashboard provides detailed information about the selected scientist, e.g. publications. The dashboard can be filtered and shows the relationship to co-authors in different diagrams. In addition, a link is provided to find contact information.

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The Materials Map is still under development. In its current state, it is only based on one single data source and, thus, incomplete and contains duplicates. We are working on incorporating new open data sources like ORCID to improve the quality and the timeliness of our data. We will update Materials Map as soon as possible and kindly ask for your patience.

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1.080 Topics available

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in Cooperation with on an Cooperation-Score of 37%

Topics

Publications (7/7 displayed)

  • 2023Graphitic C3N4 and Ti3C2 nanocomposites for the enhanced photocatalytic degradation of organic compounds and the evolution of hydrogen under visible irradiation2citations
  • 2021Photocatalytic water splitting over CeO2/Fe2O3/Ver photocatalysts30citations
  • 2020Influence of High Temperature Synthesis on the Structure of Graphitic Carbon Nitride and Its Hydrogen Generation Ability74citations
  • 2014ZnS/MMT nanocomposites : the effect of ZnS loading in MMT on the photocatalytic reduction of carbon dioxide51citations
  • 2014Photocatalytic and photochemical decomposition of N2O on ZnS-MMT Catalyst22citations
  • 2011CdS nanoparticles deposited on montmorillonite: preparation, characterization and application for photoreduction of carbon dioxide77citations
  • 2010Preparation and characterization of ZnS nanoparticles deposited on montmorillonite59citations

Places of action

Chart of shared publication
Škuta, Radim
1 / 1 shared
Edelmannová, Miroslava Filip
1 / 1 shared
Foniok, Kryštof
1 / 3 shared
Pavlovský, Jiří
1 / 1 shared
Tokarský, Jonáš
1 / 8 shared
Smýkalová, Aneta
1 / 3 shared
Praus, Petr
1 / 5 shared
Koštejn, Martin
1 / 5 shared
Reli, Martin
3 / 4 shared
Motylenko, Mykhaylo
1 / 13 shared
Čapek, Libor
2 / 2 shared
Valášková, Marta
1 / 19 shared
Ambrožová, Nela
1 / 1 shared
Schimpf, Christian
1 / 17 shared
Rafaja, David
1 / 293 shared
Edelmannová, Miroslava
2 / 2 shared
Zieliński, Michał
1 / 7 shared
Pietrowski, Mariusz
1 / 6 shared
Wojcieszak, Robert
1 / 15 shared
Alwin, Emilia
1 / 4 shared
Kotarba, Andrzej
1 / 10 shared
Praus, Petr
4 / 10 shared
Valeš, Václav
1 / 1 shared
Šafářová, Klára
1 / 2 shared
Kozák, Ondřej
3 / 4 shared
Obalová, Lucie
2 / 8 shared
Matějová, Lenka
1 / 2 shared
Šihor, Marcel
1 / 1 shared
Panáček, Aleš
1 / 2 shared
Dvorský, Richard
1 / 3 shared
Klementová, Mariana
1 / 1 shared
Chart of publication period
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Co-Authors (by relevance)

  • Škuta, Radim
  • Edelmannová, Miroslava Filip
  • Foniok, Kryštof
  • Pavlovský, Jiří
  • Tokarský, Jonáš
  • Smýkalová, Aneta
  • Praus, Petr
  • Koštejn, Martin
  • Reli, Martin
  • Motylenko, Mykhaylo
  • Čapek, Libor
  • Valášková, Marta
  • Ambrožová, Nela
  • Schimpf, Christian
  • Rafaja, David
  • Edelmannová, Miroslava
  • Zieliński, Michał
  • Pietrowski, Mariusz
  • Wojcieszak, Robert
  • Alwin, Emilia
  • Kotarba, Andrzej
  • Praus, Petr
  • Valeš, Václav
  • Šafářová, Klára
  • Kozák, Ondřej
  • Obalová, Lucie
  • Matějová, Lenka
  • Šihor, Marcel
  • Panáček, Aleš
  • Dvorský, Richard
  • Klementová, Mariana
OrganizationsLocationPeople

article

Influence of High Temperature Synthesis on the Structure of Graphitic Carbon Nitride and Its Hydrogen Generation Ability

  • Kočí, Kamila
  • Zieliński, Michał
  • Pietrowski, Mariusz
  • Wojcieszak, Robert
  • Alwin, Emilia
  • Edelmannová, Miroslava
Abstract

Graphitic carbon nitride (g-C3N4) was obtained by thermal polymerization of dicyandiamide, thiourea or melamine at high temperatures (550 and 600 °C), using different heating rates (2 or 10 °C min−1) and synthesis times (0 or 4 h). The effects of the synthesis conditions and type of the precursor on the efficiency of g-C3N4 were studied. The most efficient was the synthesis from dicyandiamide, 53%, while the efficiency in the process of synthesis from melamine and thiourea were much smaller, 26% and 11%, respectively. On the basis of the results provided by X-ray diffraction (XRD), X-ray photoelectron spectroscopy (XPS), infrared spectroscopy (FTIR), ultraviolet–visible spectroscopy (UV–vis), thermogravimetric analysis (TGA), elemental analysis (EA), the best precursor and the optimum conditions of synthesis of g-C3N4 were identified to get the product of the most stable structure, the highest degree of ordering and condensation of structure and finally the highest photocatalytic activity. It was found that as the proton concentration decreased and the degree of condensation increased, the hydrogen yields during the photocatalytic decomposition of water–methanol solution were significantly enhanced. The generation of hydrogen was 1200 µmol g−1 and the selectivity towards hydrogen of more than 98%.

Topics
  • Carbon
  • x-ray diffraction
  • x-ray photoelectron spectroscopy
  • nitride
  • Hydrogen
  • thermogravimetry
  • decomposition
  • Ultraviolet–visible spectroscopy
  • infrared spectroscopy
  • elemental analysis