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Naji, M. |
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Motta, Antonella |
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Aletan, Dirar |
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Mohamed, Tarek |
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Ertürk, Emre |
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Taccardi, Nicola |
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Kononenko, Denys |
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Petrov, R. H. | Madrid |
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Alshaaer, Mazen | Brussels |
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Bih, L. |
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Casati, R. |
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Muller, Hermance |
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Kočí, Jan | Prague |
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Šuljagić, Marija |
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Kalteremidou, Kalliopi-Artemi | Brussels |
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Azam, Siraj |
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Ospanova, Alyiya |
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Blanpain, Bart |
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Ali, M. A. |
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Popa, V. |
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Rančić, M. |
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Ollier, Nadège |
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Azevedo, Nuno Monteiro |
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Landes, Michael |
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Rignanese, Gian-Marco |
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Wysocki, Bartłomiej
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Topics
Publications (14/14 displayed)
- 2022How to Control the Crystallization of Metallic Glasses During Laser Powder Bed Fusion? Towards Part-Specific 3d Printing of in Situ Composites
- 2020Analysis of Microstructure and Properties of a Ti–AlN Composite Produced by Selective Laser Meltingcitations
- 2019The influence of chemical polishing of titanium scaffolds on their mechanical strength and in-vitro cell responsecitations
- 2019New approach to amorphization of alloys with low glass forming ability via selective laser meltingcitations
- 2018The Influence of Selective Laser Melting (SLM) Process Parameters on In-Vitro Cell Responsecitations
- 2018Investigation of the relationship between morphology and permeability for open-cell foams using virtual materials testingcitations
- 2018Structure and porosity of titanium scaffolds manufactured by selective laser meltingcitations
- 2017Microstructure and mechanical properties investigation of CP titanium processed by selective laser melting (SLM)citations
- 2017Fabrication of custom designed spinal disc replacement for veterinary applications
- 2017Laser and Electron Beam Additive Manufacturing Methods of Fabricating Titanium Bone Implantscitations
- 2016The process of design and manufacturing of titanium scaffolds in the SLM technology for tissue engineering
- 2016Post Processing and Biological Evaluation of the Titanium Scaffolds for Bone Tissue Engineeringcitations
- 2016The Novel Scanning Strategy For Fabrication Metallic Glasses By Selective Laser Melting
- 2015CNTs as ion carriers in formation of calcium phosphate coatingscitations
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article
Analysis of Microstructure and Properties of a Ti–AlN Composite Produced by Selective Laser Melting
Abstract
Selective Laser Melting (SLM) is a manufacturing technique that is currently used for the production of functional parts that are difficult to form by the traditional methods such as casting or CNC (Computer Numerical Control) cutting from a wide range of metallic materials. In our study, a mixture of commercially pure titanium (Ti) and 15% at. aluminum nitride (AlN) was Selective Laser Melted to form three-dimensional objects. The obtained 4 mm edge cubes with an energy density that varied from 70 to 140 J/mm3 were examined in terms of their microstructure, chemical and phase composition, porosity, and Vickers microhardness. Scanning Electron Microscopy (SEM) observations of the etched samples showed inhomogeneities in the form of pores and unmelted and partly melted AlN particles in the fine-grained dendritic matrix, which is typical for titanium nitrides and titanium aluminum nitrides. The AlN particles remained unmelted in samples, but no porosity was observed in the interface area between them and the dendritic matrix. Additionally, samples fabricated with the presintering step had zones with different sizes of dendrites, suggesting a differing chemical composition of the matrix and the possibility of the formation of the phases forming an Ti–Al–N ternary system. The chemical composition in the microareas of the samples was determined using Energy Dispersive X-Ray Spectroscopy (EDS) and revealed differences in the homogeneity of the samples depending on the SLM process parameters and the additional presintering step. The phase composition, examined using X-ray Diffraction analysis (XRD), showed that samples were formed from Ti, TiN, and AlN phases. Porosity tests carried out using a computer microtomography revealed porosities in a range from 7% to 17.5%. The formed material was characterized by a relatively high hardness exceeding 700 HV0.2 over the entire cross-section, which depended on the manufacturing conditions.