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Naji, M. |
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Motta, Antonella |
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Aletan, Dirar |
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Mohamed, Tarek |
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Ertürk, Emre |
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Taccardi, Nicola |
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Kononenko, Denys |
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Petrov, R. H. | Madrid |
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Alshaaer, Mazen | Brussels |
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Bih, L. |
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Casati, R. |
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Muller, Hermance |
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Kočí, Jan | Prague |
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Šuljagić, Marija |
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Kalteremidou, Kalliopi-Artemi | Brussels |
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Azam, Siraj |
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Ospanova, Alyiya |
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Blanpain, Bart |
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Ali, M. A. |
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Popa, V. |
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Rančić, M. |
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Ollier, Nadège |
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Azevedo, Nuno Monteiro |
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Landes, Michael |
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Rignanese, Gian-Marco |
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Suarez, Sebastian
in Cooperation with on an Cooperation-Score of 37%
Topics
Publications (12/12 displayed)
- 2024Modifying the Characteristics of the Electrical Arc Generated during Hot Switching by Reinforcing Silver and Copper Matrices with Carbon Nanotubes
- 2023Influence of structural depth of laser-patterned steel surfaces on the solid lubricity of carbon nanoparticle coatingscitations
- 2023Electrical Characterization of Carbon Nanotube Reinforced Silver and Copper Composites for Switching Contacts
- 2023Impact of Microstructure of Nanoscale Magnetron Sputtered Ru/Al Multilayers on Thermally Induced Phase Formationcitations
- 2023Multiwall carbon nanotubes for solid lubrication of highly loaded contactscitations
- 2023Degradation analysis of tribologically loaded carbon nanotubes and carbon onionscitations
- 2022Influence of structural depth of laser-patterned steel surfaces on the solid lubricity of carbon nanoparticle coatings
- 2020Microstructural evolution during heating of CNT/Metal Matrix Composites processed by Severe Plastic Deformation
- 2019Friction and Tribo-Chemical Behavior of SPD-Processed CNT-Reinforced Composites
- 2019Evolution of the lattice defects and crystalline domain size in carbon nanotube metal matrix composites processed by severe plastic deformation
- 2019Geometrically Necessary Dislocations on Plastic Deformation of Polycrystalline TRIP Steel
- 2018In-situ nanodiamond to carbon onion transformation in metal matrix composites
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article
Impact of Microstructure of Nanoscale Magnetron Sputtered Ru/Al Multilayers on Thermally Induced Phase Formation
Abstract
In this study, we report on phase formation and microstructure evolution in multiscale magnetron sputtered Ru/Al multilayers upon thermal annealing in vacuum at slow heating rates of 10 K/min. By specifically adjusting the microstructure and design of the as-deposited multilayers, the formation of certain desired phases can be tuned. We demonstrate that the synthesis of single phase RuAl thin films is possible in a very controlled manner in a solid state only via thermal activation without initiating the self-propagating exothermic reactions of Ru/Al multilayers. To investigate phase formation sequences and the resulting microstructures, Ru/Al multilayers were designed via magnetron sputtering with systematic variation of bilayer modulation periods and subsequent vacuum annealing. Thin films samples were characterized by in situ high-temperature XRD, TEM imaging and diffraction. It is shown that different phase sequences appear in strong correlation with the modulation length. Depending on the multilayer design, the phase formation toward single-phase RuAl thin films happens as either a multi-step or single-step event. In particular, below a critical threshold of the modulation period, the multi-step phase formation can be suppressed, and only the desired RuAl target phase is obtained with a pronounced growth in a preferred orientation. This finding may be versatile for the targeted synthesis of intermetallic phases, contributing to further understanding of phase formation in such nanoscale multilayer systems.