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| Naji, M. |
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| Mohamed, Tarek |
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| Ertürk, Emre |
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| Petrov, R. H. | Madrid |
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| Kočí, Jan | Prague |
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| Ollier, Nadège |
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| Azevedo, Nuno Monteiro |
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| Landes, Michael |
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| Rignanese, Gian-Marco |
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Zieliński, Michał
in Cooperation with on an Cooperation-Score of 37%
Topics
Publications (7/7 displayed)
- 2021Sol-Gel Approach for Design of Pt/Al2O3-TiO2 System-Synthesis and Catalytic Testscitations
- 2020Elucidating the structure of the graphitic carbon nitride nanomaterialsviaX-ray photoelectron spectroscopy and X-ray powder diffraction techniquescitations
- 2020Elucidating the structure of the graphitic carbon nitride nanomaterials using X-ray photoelectron spectroscopy and X-ray powder diffraction techniquescitations
- 2020Influence of High Temperature Synthesis on the Structure of Graphitic Carbon Nitride and Its Hydrogen Generation Abilitycitations
- 2020Elucidating the structure of the graphitic carbon nitride nanomaterials via X-ray photoelectron spectroscopy and X-ray powder diffraction techniquescitations
- 2019Structure, magnetic and catalytic properties of SiO2-MFe2O4 (M = Mn, Co, Ni, Cu) nanocomposites and their syntheses by a modified sol–gel methodcitations
- 2007Oxide phases as activators of high calorific mixture
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article
Sol-Gel Approach for Design of Pt/Al2O3-TiO2 System-Synthesis and Catalytic Tests
Abstract
Al2O3-TiO2 systems with Ti:Al 0.1, 0.5 and 1.0 molar ratio obtained by the sol–gel method have been used as a platinum support. As a precursor of alumina gel, aluminum isopropoxide has been chosen. Titanium tert-butoxylate was applied to obtain titania gel and hexachloroplatinic acid was applied as a source of platinum. The systems have been characterized by the following methods: thermogravimetric analysis (TGA), Fourier transformation infrared spectroscopy (FTIR), X-ray powder diffraction (XRPD), low-temperature nitrogen adsorption–desorption isotherms (BET, BJH), temperature-programmed reduction with hydrogen (TPR-H2) and hydrogen chemisorption. Reactions of toluene to methylcyclohexane and selective o-chloronitrobenzene (o-CNB) to o-chloroaniline (o-CAN) hydrogenation were used as the tests of systems’ catalytic activity. The application of Al2O3-TiO2 as a support has enabled the obtaining of platinum catalysts showing high activities for hydrogenation of toluene and selective hydrogenation of o-chloronitrobenzene to o-chloroaniline in the liquid phase. The highest activity in both reactions has been found for Pt/Al2O3-0.5TiO2 catalyst and the highest selectivity for Pt/Al2O3-. The activity of Pt/Al2O3-TiO2 catalysts was higher than that of alumina-supported ones