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Naji, M. |
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Motta, Antonella |
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Aletan, Dirar |
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Mohamed, Tarek |
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Ertürk, Emre |
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Taccardi, Nicola |
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Kononenko, Denys |
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Petrov, R. H. | Madrid |
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Alshaaer, Mazen | Brussels |
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Bih, L. |
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Casati, R. |
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Muller, Hermance |
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Kočí, Jan | Prague |
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Šuljagić, Marija |
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Kalteremidou, Kalliopi-Artemi | Brussels |
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Azam, Siraj |
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Ospanova, Alyiya |
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Blanpain, Bart |
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Ali, M. A. |
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Popa, V. |
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Rančić, M. |
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Ollier, Nadège |
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Azevedo, Nuno Monteiro |
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Landes, Michael |
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Rignanese, Gian-Marco |
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Petrescu, Florian Ion
in Cooperation with on an Cooperation-Score of 37%
Topics
Publications (10/10 displayed)
- 2023Photodegradation of ciprofloxacin and levofloxacin by Au@ZnONPs-MoS2-Rgo nanocompositescitations
- 2023A Comprehensive Evaluation of the Mechanical Properties of Rubberized Concretecitations
- 2022Hydrogen Production and Degradation of Ciprofloxacin by Ag@TiO2-MoS2 Photocatalystscitations
- 2019On the use of infrared thermography and acousto-ultrasonics NDT techniques for ceramic-coated sandwich structurescitations
- 2017Extended MTSN criterion for fracture analysis of soda lime glasscitations
- 2017Nano-Diamond Hybrid Materials for Structural Biomedical Applicationcitations
- 2017Influence of Curing Light Type and Staining Medium on the Discoloring Stability of Dental Restorative Compositecitations
- 2017Processability of Bulk Metallic Glassescitations
- 2016Biomechanically Inspired Shape Memory Effect Machines Driven by Muscle like Acting NiTi Alloyscitations
- 2016Glassy Amorphous Metal Injection Molded Induced Morphological Defectscitations
Places of action
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article
Hydrogen Production and Degradation of Ciprofloxacin by Ag@TiO2-MoS2 Photocatalysts
Abstract
<jats:p>The photocatalytic activity of silver-based catalysts containing different amounts of molybdenum disulfide (MoS2; 5, 10 and 20 wt.%) was evaluated by the degradation of the antibiotic ciprofloxacin and the production of hydrogen via water splitting. All the silver (Ag)-based catalysts degraded more than 70% of the antibiotic in 60 min. The catalyst that exhibited the best result was 5%Ag@TiO2-P25-5%MoS2, with ca. 91% of degradation. The control experiments and stability tests showed that photocatalysis was the degradation pathway and the selected silver-based catalysts were stable after seven cycles, with less than 2% loss of efficiency per cycle and less than 7% after seven cycles. The catalyst with the highest hydrogen production was 5%Ag@TiO2 NWs-20%MoS2, 1792 μmol/hg, at a wavelength of 400 nm. This amount was ca. 32 times greater than that obtained by the pristine titanium oxide nanowires catalyst. The enhancement was attributed to the high surface area of the catalysts, along with the synergism created by the silver nanoparticles and MoS2. All the catalysts were characterized by X-ray photoelectron spectroscopy (XPS), X-ray diffraction (XRD), Raman spectroscopy, field-emission scanning electron microscopy (FE-SEM), high-resolution transmission electron microscopy (HRTEM), Brunauer–Emmett–Teller (BET) surface area analysis and energy dispersive X-ray spectroscopy (EDS).</jats:p>