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Naji, M. |
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Motta, Antonella |
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Aletan, Dirar |
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Mohamed, Tarek |
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Ertürk, Emre |
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Taccardi, Nicola |
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Kononenko, Denys |
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Petrov, R. H. | Madrid |
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Alshaaer, Mazen | Brussels |
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Bih, L. |
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Casati, R. |
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Muller, Hermance |
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Kočí, Jan | Prague |
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Šuljagić, Marija |
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Kalteremidou, Kalliopi-Artemi | Brussels |
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Azam, Siraj |
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Ospanova, Alyiya |
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Blanpain, Bart |
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Ali, M. A. |
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Popa, V. |
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Rančić, M. |
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Ollier, Nadège |
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Azevedo, Nuno Monteiro |
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Landes, Michael |
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Rignanese, Gian-Marco |
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Dey, Dr. Avishek
University College London
in Cooperation with on an Cooperation-Score of 37%
Topics
Publications (6/6 displayed)
- 2021Tin oxide for optoelectronic, photovoltaic and energy storage devices: a reviewcitations
- 2021Removal and Degradation of Mixed Dye Pollutants by Integrated Adsorption-Photocatalysis Technique Using 2-D MoS<sub>2</sub>/TiO<sub>2</sub> Nanocompositecitations
- 2020Solution Processed Pure Sulfide CZCTS Solar Cells with Efficiency 10.8% using Ultra-Thin CuO Intermediate Layercitations
- 2019Continuous Hydrothermal Synthesis of Metal Germanates (M<sub>2</sub>GeO<sub>4</sub> ; M = Co, Mn, Zn) for High Capacity Negative Electrodes in Li‐ion Batteriescitations
- 2019Effects of Precursor Concentration in Solvent and Nanomaterials Room Temperature Aging on the Growth Morphology and Surface Characteristics of Ni–NiO Nanocatalysts Produced by Dendrites Combustion during SCScitations
- 2017Tuning the properties of a black TiO<sub>2</sub>-Ag visible light photocatalyst produced by rapid one-pot chemical reductioncitations
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article
Effects of Precursor Concentration in Solvent and Nanomaterials Room Temperature Aging on the Growth Morphology and Surface Characteristics of Ni–NiO Nanocatalysts Produced by Dendrites Combustion during SCS
Abstract
The morphology and surface characteristics of SCS(Solution Combustion Synthesis)-derived Ni−NiO nanocatalysts were studied. The ΤΕΜ results highlighted that the nanomaterial’s microstructure was modified by changing the reactants’ concentrations. The dendrites’ growth conditions were the main factors responsible for the observed changes in the nanomaterials’ crystallite size. Infrared camera measurements demonstrated a new type of combustion through dendrites. The XPS analysis revealed that the NiO structure resulted in the bridging of the oxygen structure that acted as an inhibitor of hydrogen adsorption on the catalytic surface and, consequently, the activity reduction. The RF-IGC indicated three different kinds of active sites with different energies of adsorption on the fresh catalyst and only one type on the aged catalyst. Aging of the nanomaterial was associated with changes in the microstructure of its surface by a gradual change in the chemical composition of the active centers.