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Naji, M. |
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Motta, Antonella |
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Aletan, Dirar |
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Mohamed, Tarek |
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Ertürk, Emre |
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Taccardi, Nicola |
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Kononenko, Denys |
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Petrov, R. H. | Madrid |
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Alshaaer, Mazen | Brussels |
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Bih, L. |
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Casati, R. |
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Muller, Hermance |
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Kočí, Jan | Prague |
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Šuljagić, Marija |
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Kalteremidou, Kalliopi-Artemi | Brussels |
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Azam, Siraj |
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Ospanova, Alyiya |
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Blanpain, Bart |
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Ali, M. A. |
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Popa, V. |
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Rančić, M. |
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Ollier, Nadège |
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Azevedo, Nuno Monteiro |
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Landes, Michael |
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Rignanese, Gian-Marco |
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Boukos, Nikos
in Cooperation with on an Cooperation-Score of 37%
Topics
Publications (6/6 displayed)
- 2023In Tandem Control of La-Doping and CuO-Heterojunction on SrTiO3 Perovskite by Double-Nozzle Flame Spray Pyrolysis: Selective H2 vs. CH4 Photocatalytic Production from H2O/CH3OHcitations
- 2023Covalently Modified Kevlar Fabric Incorporating Graphene Oxide with Enhanced Antibacterial Properties and Preserved Strengthcitations
- 2023Kevlar®, Nomex®, and VAR Modification by Small Organic Molecules Anchoring: Transfusing Antibacterial Properties and Improving Water Repellencycitations
- 2019Effects of Precursor Concentration in Solvent and Nanomaterials Room Temperature Aging on the Growth Morphology and Surface Characteristics of Ni–NiO Nanocatalysts Produced by Dendrites Combustion during SCScitations
- 2019Effects of Precursor Concentration in Solvent and Nanomaterials Room Temperature Aging on the Growth Morphology and Surface Characteristics of Ni–NiO Nanocatalysts Produced by Dendrites Combustion during SCScitations
- 2014Atomic-layer-deposited aluminum and zirconium oxides for surface passivation of TiO 2 in high-efficiency organic photovoltaicscitations
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article
Effects of Precursor Concentration in Solvent and Nanomaterials Room Temperature Aging on the Growth Morphology and Surface Characteristics of Ni–NiO Nanocatalysts Produced by Dendrites Combustion during SCS
Abstract
The morphology and surface characteristics of SCS(Solution Combustion Synthesis)-derived Ni−NiO nanocatalysts were studied. The ΤΕΜ results highlighted that the nanomaterial’s microstructure was modified by changing the reactants’ concentrations. The dendrites’ growth conditions were the main factors responsible for the observed changes in the nanomaterials’ crystallite size. Infrared camera measurements demonstrated a new type of combustion through dendrites. The XPS analysis revealed that the NiO structure resulted in the bridging of the oxygen structure that acted as an inhibitor of hydrogen adsorption on the catalytic surface and, consequently, the activity reduction. The RF-IGC indicated three different kinds of active sites with different energies of adsorption on the fresh catalyst and only one type on the aged catalyst. Aging of the nanomaterial was associated with changes in the microstructure of its surface by a gradual change in the chemical composition of the active centers.