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Naji, M. |
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Motta, Antonella |
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Aletan, Dirar |
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Mohamed, Tarek |
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Ertürk, Emre |
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Taccardi, Nicola |
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Kononenko, Denys |
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Petrov, R. H. | Madrid |
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Alshaaer, Mazen | Brussels |
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Bih, L. |
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Casati, R. |
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Muller, Hermance |
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Kočí, Jan | Prague |
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Šuljagić, Marija |
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Kalteremidou, Kalliopi-Artemi | Brussels |
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Azam, Siraj |
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Ospanova, Alyiya |
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Blanpain, Bart |
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Ali, M. A. |
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Popa, V. |
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Rančić, M. |
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Ollier, Nadège |
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Azevedo, Nuno Monteiro |
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Landes, Michael |
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Rignanese, Gian-Marco |
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Fisslthaler, Evelin
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Publications (7/7 displayed)
- 2024Challenges and advances regarding LiVPO4: From HR-STEM & EELS to novel scanning diffraction techniques
- 20232D and 3D STEM Imaging and Spectroscopy: Applications and Perspectives in View of Novel STEM Infrastructure
- 2023Influence of growth temperature on the properties of aluminum nitride thin films prepared by magnetron sputter epitaxycitations
- 2023AlYN Thin Films with High Y Content: Microstructure and Performancecitations
- 2022Challenges in the characterization of complex nanomaterials with analytical STEM
- 2021Spectroscopic STEM imaging in 2D and 3D
- 2013TEM Sample Preparation of a Hard Metal by Semiautomatic Wedge Polishing
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article
TEM Sample Preparation of a Hard Metal by Semiautomatic Wedge Polishing
Abstract
<jats:title>Abstract</jats:title><jats:p>Sintered hard metals like tungsten carbide compounds are a challenge for TEM sample preparation due to the diverging properties of the individual components. Especially when both very thin as well as large areas are required, for example for nanoanalysis investigations, conventional preparation techniques like ion milling and FIB preparation are often incapable of delivering samples of necessary quality. In this study, the preparation of a hard metal consisting of a tungsten carbide/cobalt compound via a technique called “Wedge Polishing” is described, along with the results of concomitant TEM investigations. The impact of the preparation procedure on the crystallographic structure of the material is discussed, and a post-treatment process to dispose of these artefacts is presented.</jats:p>