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Naji, M. |
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Motta, Antonella |
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Aletan, Dirar |
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Mohamed, Tarek |
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Ertürk, Emre |
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Taccardi, Nicola |
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Kononenko, Denys |
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Petrov, R. H. | Madrid |
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Alshaaer, Mazen | Brussels |
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Bih, L. |
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Casati, R. |
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Muller, Hermance |
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Kočí, Jan | Prague |
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Šuljagić, Marija |
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Kalteremidou, Kalliopi-Artemi | Brussels |
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Azam, Siraj |
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Ospanova, Alyiya |
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Blanpain, Bart |
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Ali, M. A. |
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Popa, V. |
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Rančić, M. |
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Ollier, Nadège |
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Azevedo, Nuno Monteiro |
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Landes, Michael |
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Rignanese, Gian-Marco |
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Mangelinck-Noël, Nathalie
Laboratoire de Mécanique et Procédés de Fabrication
in Cooperation with on an Cooperation-Score of 37%
Topics
Publications (57/57 displayed)
- 2022Microstructure Analysis of Al-7 wt% Si Alloy Solidified on Earth Compared to Similar Experiments in Microgravitycitations
- 2022Concurrent model for sharp and progressive columnar to equiaxed transitions validated by directional solidification experiments processed in microgravity conditionscitations
- 2022Influence of Solidification Parameters on the Amount of Eutectic and Secondary Arm Spacing of Al-7wt% Si Alloy Solidified under Microgravitycitations
- 2021Analysis of gravity effects during binary alloy directional solidification by comparison of microgravity and Earth experiments with in situ observationcitations
- 2020Modification of the microstructure by rotating magnetic field during the solidification of Al-7 wt.% Si alloy under microgravitycitations
- 2020Investigation of subgrains in directionally solidified cast mono-seeded silicon and their interactions with twin boundariescitations
- 2019Comparative study of directional solidification of Al-7 wt% Si alloys in Space and on Earth: Effects of gravity on dendrite growth and Columnar-to-equiaxed transition
- 2019Comparative study of directional solidification of Al-7 wt% Si alloys in Space and on Earth: Effects of gravity on dendrite growth and Columnar-to-equiaxed transition
- 2019Role of Impurities in Silicon Solidification and Electrical Properties Studied by Complementary in Situ and Ex Situ Methodscitations
- 2017Impact of the Seed Layer Morphology on the Initial Growth of HPMC-Si Ingotcitations
- 2017Columnar and Equiaxed Solidification of Al-7 wt.% Si Alloys in Reduced Gravity in the Framework of the CETSOL Projectcitations
- 2016Convection and solidification influenced by thermo-electric effect
- 2016Convection and solidification influenced by thermo-electric effect
- 2015Microstructural development and mechanical properties of a near-eutectic directionally solidified Sn–Bi solder alloycitations
- 2015Cooling thermal parameters, microstructure, segregation and hardness in directionally solidified Al–Sn-(Si;Cu) alloyscitations
- 2015Simulation of directional solidification of refined Al–7wt.%Si alloys – Comparison with benchmark microgravity experimentscitations
- 2015Motion of equiaxed grains during directional solidification under static magnetic field
- 2014Structures in directionally solidified Al-7 wt.% Si alloys: Benchmark experiments under microgravitycitations
- 2014In Situ Investigation of Dendrite Deformation During Upward Solidification of Al-7wt.%Sicitations
- 2014Magnetic Fields, Convection and Solidificationcitations
- 2014Magnetic Fields, Convection and Solidificationcitations
- 2014In Situ and Real-Time Analysis of TEM Forces Induced by a Permanent Magnetic Field during Solidification of Al-4wt%Cucitations
- 2014Coupled Cellular Automaton (CA) - Finite Element (FE) Modeling of Directional Solidification of Al-3.5 wt% Ni Alloy: A Comparison with X-ray Synchrotron Observationscitations
- 2014CAFE simulation of columnar-to-equiaxed transition in Al-7wt%Si alloys directionally solidified under microgravitycitations
- 2014Columnar-to-equiaxed transition in solidification processing of ALSi7 alloys in microgravity-the CETSOL projectcitations
- 2013Influence of natural convection during upward directional solidification: A comparison between in situ X-ray radiography and direct simulation of the grain structurecitations
- 2012Direct simulation of a directional solidification experiment observed in situ and real-time using X-ray imagingcitations
- 2012CET during the solidification of refined Al-3.5wt%Ni alloys and characterization of the subsequent grain structurecitations
- 2011Analysis by synchrotron X-ray radiography of convection effects on the dynamic evolution of the solid–liquid interface and on solute distribution during the initial transient of solidificationcitations
- 2011In situ and real-time analysis of the growth and interaction of equiaxed grains by synchrotron X- ray radiographycitations
- 2010Al–Fe hypoeutectic alloys directionally solidified under steady-state and unsteady-state conditionscitations
- 2010Measurement of Solute Profiles by Means of Synchrotron X-Ray Radiography during Directional Solidification of Al-4 wt% Cu Alloyscitations
- 2010In Situ Synchrotron X-ray Characterization of Microstructure Formation in Solidification Processing of Al-based Metallic Alloyscitations
- 2010Influence of forced/natural convection on segregation during the directional solidification of Al-based binary alloys.
- 2009In situ analysis of dendritic equiaxed microstructure formation in Al-Cu alloys by synchrotron X-ray radiographycitations
- 2009Directional solidification processing on CET in Al-based alloyscitations
- 2009Columnar to equiaxed transition during directional solidification in refined Al-based alloyscitations
- 2008Modeling of heat and solute interactions upon grain structure solidificationcitations
- 2008In situ and real-time analysis of TGZM phenomena by synchrotron X-ray radiographycitations
- 2007In-Situ and Real-Time Investigation of Columnar-to-Equiaxed Transition in Metallic Alloycitations
- 2007In situ study of the quasicrystal growth by synchrotron X-ray imagingcitations
- 2007Control of melt convection by a travelling magnetic field during the directional solidification of Al–Ni alloyscitations
- 2007Real-time and in situ solidification of Al-based alloys investigated by synchrotron radiation: a unique experimental set-up combining radiography and topography techniquescitations
- 2007Growth Structures, Interface Dynamics and Stresses in Metallic Alloy Solidification: In situ Synchrotron X-ray Characterisation
- 2006In situ and real time investigation of directional solidification of Al-Ni alloys by synchrotron imagingcitations
- 2006Studies by In Situ and Real-Time Synchrotron Imaging of Interface Dynamics and Defect Formation in Solidification Processingcitations
- 2006Studies by In Situ and Real-Time Synchrotron Imaging of Interface Dynamics and Defect Formation in Solidification Processingcitations
- 2006Effect of Travelling Magnetic Field on the Directional Solidification of refined Al-3.5 wt %Ni alloys
- 2006Effect of Travelling Magnetic Field on the Directional Solidification of refined Al-3.5 wt %Ni alloys
- 2005Investigation of columnar–equiaxed transition and equiaxed growth of aluminium based alloys by X-ray radiography
- 2005Necessity of investigating microstructure formation during directional solidification of transparent alloys in 3Dcitations
- 2005Effects of the interface curvature on cellular and dendritic microstructurescitations
- 2005Application of synchrotron X-ray imaging to the study of directional solidification of aluminium-based alloyscitations
- 2005Grain size reduction by electromagnetic stirring inside gold alloys
- 2004Columnar-to-Equiaxed Transition in SOLidification Processing (CETSOL): a project of the European Space Agency (ESA) - Microgravity Applications Promotion (MAP) programmecitations
- 2003MODELING THE MULTI-CRYSTALLINE SILICON INGOT SOLIDIFICATION PROCESS IN A VERTICAL SQUARE FURNACE
- 2000Optical device dedicated to the non-destructive observation and characterization of the solidification of bulk transparent alloys in situ and in real time
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article
In Situ Synchrotron X-ray Characterization of Microstructure Formation in Solidification Processing of Al-based Metallic Alloys
Abstract
The microstructure formed during the solidification step has a major influence on the properties of materials processed by major techniques (casting, welding . . . ). In situ and real-time characterization by synchrotron X-ray imaging is the method of choice to unveil the dynamical formation of the solidification microstructure in metallic alloys, and thus provide precise data for the critical validation of the theoretical predictions that is needed for sound advancement of modeling and numerical simulation. After a description of the experimental procedure used at the European Synchrotron Radiation Facility (ESRF), dynamical phenomena in the formation of the grain structure and dendritic or equiaxed solidification microstructure in Al-based alloys are presented. Beyond fluid flow interaction, earth gravity induces stresses, deformation and fragmentation in the dendritic mush. Settling of dendrite arms and equiaxed grains thus occurs, in particular in the columnar to equiaxed transition. Other types of stresses and strains are caused by the mere formation of the solidification microstructure itself. In white-beam X-ray topography, stresses and strains are manifested by specific contrasts and breaking of the Laue images into several pieces. Finally, quantitative analysis of the grey level in radiographs enables the analysis of solute segregation, which noticeably results in solutal poisoning of growth when equiaxed grains are interacting.