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Naji, M. |
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Motta, Antonella |
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Aletan, Dirar |
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Mohamed, Tarek |
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Ertürk, Emre |
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Taccardi, Nicola |
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Kononenko, Denys |
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Petrov, R. H. | Madrid |
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Alshaaer, Mazen | Brussels |
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Bih, L. |
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Casati, R. |
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Muller, Hermance |
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Kočí, Jan | Prague |
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Šuljagić, Marija |
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Kalteremidou, Kalliopi-Artemi | Brussels |
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Azam, Siraj |
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Ospanova, Alyiya |
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Blanpain, Bart |
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Ali, M. A. |
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Popa, V. |
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Rančić, M. |
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Ollier, Nadège |
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Azevedo, Nuno Monteiro |
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Landes, Michael |
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Rignanese, Gian-Marco |
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Mihajlović, Slavica
in Cooperation with on an Cooperation-Score of 37%
Topics
Publications (17/17 displayed)
- 2024The influence of high compaction pressure on cordierite-based ceramics
- 2023X-ray structural analysis of the BaO and TiO2 starting compounds and initial mechanochemical activation
- 2023Mechanochemical synthesis of strontium titanate
- 2023Microstructure assessment of co alloy intended for dentistry
- 2022Fourier-transform infrared spectroscopy analysis of mechanochemical transformation kinetics of sodium carbonate to bicarbonatecitations
- 2022Possibility of obtaining magnesium titanate by mechanochemical process in a high-energy vibro mill
- 2022Examination of influence sintering temperature on mineral compounds
- 2021X-ray diffraction and SEM analysis of waste sulfur modification for use in concretescitations
- 2021XRD analysis of activated four-component ceramics
- 2021The influence of high compaction pressure on cordierite-based ceramics
- 2021Influence of sintering time on density properties and SEM analysis of cordierite-based ceramics
- 2021SEM and X-ray analyses of sintered MgO/Bi2O3 binary system
- 2021Electrical properties of isothermally sintered cordierite-based ceramics as funcion of sintering and activation time
- 2020Influence of mechanochemical activation on components on synthesis of cordierite ceramics for application in electronics
- 2020Impact of relaxation time of activated mixture on ceramics synthesis for electronic purposes
- 2019Potential ways to lower CO2 emission for cement production
- 2015Investigation of the application of the natural and with lead ions contaminated zeolite as an addition in portland cement
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article
Fourier-transform infrared spectroscopy analysis of mechanochemical transformation kinetics of sodium carbonate to bicarbonate
Abstract
<jats:p>During mechanical activation, qualitative changes that can produce variousphenomena occur in the material. In this study, anhydrous sodium carbonatewas mechanically activated for 2, 7, 14, and 28 minutes in a vibro mill at afrequency of 3000 oscillations per minute. After activation, four series ofactivated samples were stored in the air at room conditions for 31 days(relaxation period). To monitor the kinetics of the transformation processof activated sodium carbonate samples, i.e. the mechanism of sodiumbicarbonate formation during relaxation, Fourier-transform infrared (FTIR)spectroscopy analysis was used. FTIR testing was performed as a function ofrelaxation time for all four series of samples, with characteristic groupsobserved: CO32-, HCO3- and OH-. The obtained results provided kineticsparameters for the transformation of sodium carbonate into sodiumbicarbonate due to the chemisorption of moisture and carbon dioxide from theatmosphere.</jats:p>