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Naji, M. |
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Motta, Antonella |
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Aletan, Dirar |
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Mohamed, Tarek |
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Ertürk, Emre |
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Taccardi, Nicola |
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Kononenko, Denys |
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Petrov, R. H. | Madrid |
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Alshaaer, Mazen | Brussels |
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Bih, L. |
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Casati, R. |
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Muller, Hermance |
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Kočí, Jan | Prague |
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Šuljagić, Marija |
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Kalteremidou, Kalliopi-Artemi | Brussels |
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Azam, Siraj |
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Ospanova, Alyiya |
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Blanpain, Bart |
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Ali, M. A. |
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Popa, V. |
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Rančić, M. |
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Ollier, Nadège |
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Azevedo, Nuno Monteiro |
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Landes, Michael |
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Rignanese, Gian-Marco |
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Schoenstein, Frédéric
Université Sorbonne Paris Nord
in Cooperation with on an Cooperation-Score of 37%
Topics
Publications (24/24 displayed)
- 2023Microstructure effects on thermal and electrical conductivities in the intermetallic compound Ag$$_{3}$$Sn-based materials, sintered by SPS in view of die-attachment applicationscitations
- 2023Grain-size effect on Cr3+ and F-centres photoluminescence in nanophase MgAl2O4 ceramicscitations
- 2023Grain-size effect on Cr$^{3+}$ and F-centres photoluminescence in nanophase MgAl$_2$O$_4$ ceramicscitations
- 2022Spark Plasma Sintering of Nanostructured TiCrC Carbides Prepared via Mechanical Alloyingcitations
- 2022The Polyol Process and the Synthesis of ζ Intermetallic Compound Ag5Sn0.9citations
- 2020From Ni–P Metastable Alloy Nanoparticles to Bulk Submicrometer Grain-Sized MMCs with Tunable Mechanical and Magnetic Propertiescitations
- 2020Spin Coating and Micro-Patterning Optimization of Composite Thin Films Based on PVDFcitations
- 2020Enhanced Magnetic Behavior of Cobalt Nano-Rods Elaborated by the Polyol Process Assisted with an External Magnetic Fieldcitations
- 2019Morphology and luminescence of MgAl2O4 ceramics obtained via spark plasma sinteringcitations
- 2018Composite microstructures and piezoelectric properties in tantalum substituted lead-free K 0.5 Na 0.5 Nb 1-x Ta x O 3 ceramicscitations
- 2017Substitution effect of Me = Al, Bi, Cr and Mn to the microwave properties of polyaniline/BaMeFe 11 O 19 for absorbing electromagnetic wavescitations
- 2017Spark plasma sintering (SPS) of pure and doped alumina ceramics
- 2017Effect of stacking faults on the magnetocrystalline anisotropy of hcp Co-based nanowirescitations
- 2015Synthesis, microstructure and electromechanical properties of undoped (K0·5Na0·5)NbO3citations
- 2014Nanocrystalline Hydroxyapatite Ceramics Prepared by Hydrolysis in Polyol Medium, Microstructure and Mechanical Properties after Spark Plasma Sintering.citations
- 2014Spark Plasma Sintering constrained process parameters of sintered silver paste for connection in power electronic modules: Microstructure, mechanical and thermal propertiescitations
- 2014The effect of pH and the process of direct or inverse synthesis of silicon-Substituted hydroxyapatite prepared by hydrolysis in aqueous medium.citations
- 2014Piezoelectric performances of undoped (K,Na)NbO3 ceramics and crystals for transducers applications. citations
- 2014Effect of spark plasma sintering process on the microstructure and mechanical properties of Nano crystalline hydroxyapatite ceramics prepared by hydrolysis in polyol mediumcitations
- 2014Effect of spark plasma sintering process on the microstructure and mechanical properties of Nano crystalline hydroxyapatite ceramics prepared by hydrolysis in polyol mediumcitations
- 2014Electromechanical Properties and Microstructure of Undoped K0.5Na0.5NbO3 Ceramics and KNbO3-NaNbO3 Crystalscitations
- 2014High electromechanical performance with spark plasma sintering of undoped K0.5Na0.5NbO3 ceramicscitations
- 2013Synthesis and functional properties of piezoelectric lead free K0.5Na0.5NbO3 ceramics and single crystals.
- 2007CoFe2O4 NANOSTRUCTURED MAGNETIC MATERIALS : INFLUENCE OF NOT-CONVENTIONAL METHODS OF COMPACTION (SPS, HIP) ON THE MICROSTRUCTURE AND PHYSICAL CHARACTERISTICS.
Places of action
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document
Spark Plasma Sintering of Nanostructured TiCrC Carbides Prepared via Mechanical Alloying
Abstract
<jats:p>In order to produce nanostructured Ti0.9Cr0.1C powders, an elemental powder mixture of titanium, chromium, and graphite is milled in this work using a high-energy ball mill for various milling times. Microstructural characteristics such as crystallite size, microstrain, lattice parameter, and dislocation density are determined using X-ray diffraction (XRD). Mechanical alloying successfully produced nanocrystalline (Ti,Cr)C with an average crystallite size of 11 nm. This size of the crystallites is also directly verified using transmission electron microscopy (TEM). Scanning electron microscopy (SEM) was used to investigate the morphology of the samples. The novelty of this work is advancing the scientific understanding of the effect of milling time on the particle size distribution and crystalline structure, and also understanding the effect of the spark plasma sintering on the different properties of the bulks. Densified cermet samples were produced from the nanocrystalline powders, milled for 5, 10 and 20 hours by SPS process at 1800 degrees for 5 min under a pressure of 80 MPa. Phase changes of the produced cermets were examined according to XRD, SEM/EDX analyses. Significant amounts of Cr and Fe elements were detected, especially in the 20 h milled cermet. The bulk forms of the milled powders for 5 and 20 h had a relative density of 98.43 and 98.51 %, respectively. However, 5 h milled cermet had 93.3 HRA because of the more homogeneous distribution of the (Ti,Cr)C phase, the low iron content and high relative density. According to the 0.0011 mm/year corrosion rate, and 371.68 k&Omega;*cm2 charge transfer resistance obtained from the potentiodynamic polarization and EIS tests, the 20 h cermet was the specimen with the highest corrosion resistance.</jats:p>