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Naji, M. |
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Motta, Antonella |
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Aletan, Dirar |
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Mohamed, Tarek |
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Ertürk, Emre |
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Taccardi, Nicola |
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Kononenko, Denys |
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Petrov, R. H. | Madrid |
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Alshaaer, Mazen | Brussels |
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Bih, L. |
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Casati, R. |
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Muller, Hermance |
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Kočí, Jan | Prague |
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Šuljagić, Marija |
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Kalteremidou, Kalliopi-Artemi | Brussels |
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Azam, Siraj |
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Ospanova, Alyiya |
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Blanpain, Bart |
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Ali, M. A. |
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Popa, V. |
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Rančić, M. |
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Ollier, Nadège |
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Azevedo, Nuno Monteiro |
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Landes, Michael |
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Rignanese, Gian-Marco |
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Manke, Ingo
Helmholtz-Zentrum Berlin für Materialien und Energie
in Cooperation with on an Cooperation-Score of 37%
Topics
Publications (26/26 displayed)
- 2024R‐Vine Copulas for Data‐Driven Quantification of Descriptor Relationships in Porous Materialscitations
- 2024Opportunities and Challenges of Calendering Sulfide‐Based Separators for Solid‐State Batteriescitations
- 2023Roadmap for focused ion beam technologiescitations
- 2023Roadmap for focused ion beam technologiescitations
- 2023Torsion of a rectangular bar: Complex phase distribution in 304L steel revealed by neutron tomography
- 2023Unveiling the impact of cross-linking redox-active polymers on their electrochemical behavior by 3D imaging and statistical microstructure analysiscitations
- 2023Spectral neutron tomography
- 20223D microstructure characterization of polymer battery electrodes by statistical image analysis based on synchrotron X-ray tomographycitations
- 2022Temperature dependence in Bragg edge neutron transmission measurementscitations
- 2022Phosphonated graphene oxide-modified polyacrylamide hydrogel electrolytes for solid-state zinc-ion batteriescitations
- 2022Quantification of Hydrogen in Metals Applying Neutron Imaging Techniques
- 2022Fabrication and characterization of porous mullite ceramics derived from fluoride-assisted Metakaolin-Al(OH)3 annealing for filtration applications
- 2021Lithium deposition in single-ion conducting polymer electrolytescitations
- 2021Stochastic 3D microstructure modeling of anodes in lithium-ion batteries with a particular focus on local heterogeneitycitations
- 2021Hierarchical Structuring of NMC111-Cathode Materials in Lithium-Ion Batteries: An In-Depth Study on the Influence of Primary and Secondary Particle Sizes on Electrochemical Performance
- 2020Performance and behavior of LLZO-based composite polymer electrolyte for lithium metal electrode with high capacity utilizationcitations
- 2020Hierarchical Structuring of NMC111-Cathode Materials in Lithium-Ion Batteries: An In-Depth Study on the Influence of Primary and Secondary Particle Sizes on Electrochemical Performancecitations
- 2020X‐Ray‐Computed Radiography and Tomography Study of Electrolyte Invasion and Distribution inside Pristine and Heat‐Treated Carbon Felts for Redox Flow Batteries
- 2020Hierarchical Structuring of NMC111-Cathode Materials in Lithium-Ion Batteriescitations
- 2019On a pluri-Gaussian model for three-phase microstructures, with applications to 3D image data of gas-diffusion electrodescitations
- 2019In Operando Neutron Radiography Analysis of a High-Temperature Polymer Electrolyte Fuel Cell Based on a Phosphoric Acid-Doped Polybenzimidazole Membrane Using the Hydrogen-Deuterium Contrast Method
- 2019X‐ray‐computed radiography and tomography study of electrolyte invasion and distribution inside pristine and heat‐treated carbon felts for redox flow batteries
- 2018Correlating Morphological Evolution of Li Electrodes with Degrading Electrochemical Performance of Li/LiCoO2 and Li/S Battery Systemscitations
- 2016Filling in the gaps
- 2015How mobile are protons in the structure of dental glass ionomer cements?citations
- 2013Methodology for Combined Neutron Diffraction and Bragg Edge Imagingcitations
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article
Methodology for Combined Neutron Diffraction and Bragg Edge Imaging
Abstract
<jats:title>ABSTRACT</jats:title><jats:p>Simultaneous use of neutron diffraction and attenuation based transmission Bragg edge imaging for strain measurements is demonstrated in this paper using the pulse neutron source at Los Alamos National Laboratory. Cylindrical samples made from ferritic steel have been subjected to <jats:italic>in-situ</jats:italic> elastic loading in tension and torsion. Lattice strains were investigated for both deformation modes by time-of-flight (TOF) neutron diffraction using two detector banks at 2θ of ±90°. At the same time, the transmitted portion of the neutron beam was recorded with the goal to analyze the position and shape of the Bragg edges, using a novel time/energy resolved Microchannel Plate (MCP) detector with pixel size of 55 µm and a 28x28 mm<jats:sup>2</jats:sup> field of view. Lattice strains obtained using neutron diffraction indicate that the deformation path (tension versus torsion) has important effect on their evolution and related results are summarized.</jats:p><jats:p>The emphasis of this paper is to explain the aspects of the experimental setup and data interpretation associated with neutron Bragg edge transmission technique for obtaining through-thickness averaged strain measurements. Implications of using transmission imaging based strain mapping for samples subjected to deformation under tensile loading (where stress at a given cross-section is constant) versus torsional loading (where stress varies linearly from center to outer radius) are discussed. In the case of samples subjected to tensile loading, analysis of the Bragg edge shifts provides the strain value in the direction of the transmitted beam. Thus, three strain components are measured simultaneously when performing Bragg edge imaging in addition to diffraction using two detector banks. For specimens subjected to pure shear by torsion, the Bragg edge transmission technique cannot readily provide quantitative strain information as the mid-point of the Bragg edge does not shift uniformly due to external loading, but results in a broadening of the Bragg edge. Such information can be used to describe the variation of strain distribution along the transmitted beam direction. Spatially resolved Bragg edge maps will be very helpful to detect d-spacing inhomogeneities within the illuminated volume, which may remain undetected when using diffraction only measurements.</jats:p>