Materials Map

Discover the materials research landscape. Find experts, partners, networks.

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The Materials Map is an open tool for improving networking and interdisciplinary exchange within materials research. It enables cross-database search for cooperation and network partners and discovering of the research landscape.

The dashboard provides detailed information about the selected scientist, e.g. publications. The dashboard can be filtered and shows the relationship to co-authors in different diagrams. In addition, a link is provided to find contact information.

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The Materials Map is still under development. In its current state, it is only based on one single data source and, thus, incomplete and contains duplicates. We are working on incorporating new open data sources like ORCID to improve the quality and the timeliness of our data. We will update Materials Map as soon as possible and kindly ask for your patience.

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Naji, M.
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Ni, N.

  • Google
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Imperial College London

in Cooperation with on an Cooperation-Score of 37%

Topics

Publications (25/25 displayed)

  • 2017Micromechanical strength of individual Al2O3 platelets42citations
  • 2017The use of 3d graphene networks for the creation of bio-inspired self-monitoring tough ceramic nanocompositescitations
  • 2017High-Mobility and High-Optical Quality Atomically Thin WS294citations
  • 2016Porosity in oxides on zirconium fuel cladding alloys, and its importance in controlling oxidation rates111citations
  • 2016An investigation of the oxidation behaviour of zirconium alloys using isotopic tracers and high resolution SIMS57citations
  • 2016How the crystallography and nanoscale chemistry of the metal/oxide interface develops during the aqueous oxidation of zirconium cladding alloys139citations
  • 2016Multi-scale characterisation of oxide on zirconium alloys6citations
  • 2016Mechanisms of oxidation of fuel cladding alloys revealed by high resolution APT, TEM and SIMS analysis8citations
  • 2016Focussed ion beam sectioning for the 3D characterisation of cracking in oxide scales formed on commercial ZIRLO (TM) alloys during corrosion in high temperature pressurised water90citations
  • 2016Studies regarding corrosion mechanisms in zirconium alloys36citations
  • 2016The atomic scale structure and chemistry of the zircaloy-4 metal-oxide interfacecitations
  • 20163D visualisation of crack distributions in oxidised zirconium alloys by FIB-slicing1citations
  • 2016Characterizing environmental degradation in PWRs by 3D FIB sequential sectioningcitations
  • 2016Quantitative EELS analysis of zirconium alloy metal/oxide interfaces.63citations
  • 2016Crystal structure of the zro phase at zirconium/zirconium oxide interfaces84citations
  • 2015The effect of Sn on corrosion mechanisms in advanced Zr-cladding for pressurised water reactors9citations
  • 2014Effect of Sn on Corrosion Mechanisms in Advanced Zr-Cladding for Pressurised Water Reactors9citations
  • 2013An investigation of the oxidation behaviour of zirconium alloys using isotopic tracers and high resolution SIMS57citations
  • 2013An investigation of the oxidation behaviour of zirconium alloys using isotopic tracers and high resolution SIMS57citations
  • 2013The effect of Sn on corrosion mechanisms in advanced Zr-cladding for pressurised water reactorscitations
  • 2012How the crystallography and nanoscale chemistry of the metal/oxide interface develops during the aqueous oxidation of zirconium cladding alloys139citations
  • 2012How the crystallography and nanoscale chemistry of the metal/oxide interface develops during the aqueous oxidation of zirconium cladding alloys139citations
  • 2012Mechanisms of oxidation of fuel cladding alloys revealed by high resolution APT, TEM and SIMS analysis8citations
  • 2011Studies regarding corrosion mechanisms in zirconium alloys36citations
  • 2011Studies regarding corrosion mechanisms in zirconium alloys36citations

Places of action

Chart of shared publication
Giuliani, F.
1 / 19 shared
Saiz, E.
2 / 15 shared
Vandeperre, L.
1 / 7 shared
Giovannini, T.
1 / 1 shared
Ferraro, C.
2 / 6 shared
Feilden, E.
1 / 4 shared
Picot, O. T.
1 / 5 shared
Saunders, T.
1 / 4 shared
Meille, S.
1 / 7 shared
Chevalier, J.
1 / 22 shared
Rocha, V. G.
1 / 4 shared
Peijs, Ton
1 / 237 shared
Reece, M. J.
1 / 22 shared
Delia, E.
1 / 5 shared
Reale, F.
1 / 1 shared
Amit, I.
1 / 1 shared
Palczynski, P.
1 / 2 shared
Sherrell, Pc
1 / 1 shared
Agnoli, S.
1 / 12 shared
Craciun, Mf
1 / 5 shared
Jones, Gf
1 / 1 shared
Mehew, Jd
1 / 2 shared
Mattevi, C.
1 / 5 shared
Russo, S.
1 / 16 shared
Bacon, A.
1 / 2 shared
Sykes, J.
12 / 14 shared
Grovenor, C.
14 / 81 shared
Jenkins, M.
1 / 13 shared
Lozano-Perez, S.
22 / 81 shared
English, C.
5 / 7 shared
Smith, G.
9 / 40 shared
Yardley, S.
4 / 4 shared
Lyon, S.
9 / 16 shared
Preuss, M.
8 / 83 shared
Moore, K.
3 / 10 shared
Wei, J.
10 / 19 shared
Wang, P.
6 / 34 shared
Cottis, R.
3 / 4 shared
Hudson, D.
9 / 15 shared
Storer, S.
3 / 3 shared
Chong, K.
1 / 2 shared
Polatidis, E.
3 / 23 shared
Fitzpatrick, M.
2 / 3 shared
Comstock, R.
1 / 2 shared
Ambard, A.
6 / 20 shared
Blat-Yrieix, M.
6 / 7 shared
Frankel, P.
3 / 18 shared
Cottis, B.
3 / 3 shared
Smith, J.
4 / 17 shared
Hallstadius, L.
6 / 16 shared
Saxey, D.
1 / 11 shared
Hughes, G.
1 / 14 shared
Terachi, T.
1 / 10 shared
Yamada, T.
1 / 19 shared
Kruska, K.
1 / 7 shared
Mccomb, D.
1 / 1 shared
Nicholls, R.
1 / 6 shared
Nellist, P.
1 / 14 shared
London, A.
1 / 4 shared
Yates, Jr
1 / 7 shared
Pickard, C.
1 / 2 shared
Moat, R.
1 / 5 shared
Forsey, A.
3 / 4 shared
Frankel, P. G.
2 / 4 shared
Comstock, R. J.
3 / 12 shared
Preuss, Michael
1 / 101 shared
Cottis, R. A.
3 / 12 shared
Grovenor, Crm
1 / 21 shared
Francis, E. M.
2 / 5 shared
Grovenor, C. R. M.
7 / 18 shared
Moat, Richard J.
2 / 33 shared
Moore, Kl
3 / 21 shared
Lyon, Stuart B.
3 / 56 shared
Wei, J. F.
2 / 2 shared
Yardley, S. S.
6 / 6 shared
Moore, K. L.
3 / 6 shared
Francis, E.
1 / 3 shared
Smith, G. D. W.
3 / 9 shared
Sykes, J. M.
3 / 3 shared
Frankel, Philipp
1 / 73 shared
Comstock, B.
2 / 2 shared
Chong, K. B.
2 / 4 shared
Fitzpatrick, M. E.
1 / 20 shared
Chart of publication period
2017
2016
2015
2014
2013
2012
2011

Co-Authors (by relevance)

  • Giuliani, F.
  • Saiz, E.
  • Vandeperre, L.
  • Giovannini, T.
  • Ferraro, C.
  • Feilden, E.
  • Picot, O. T.
  • Saunders, T.
  • Meille, S.
  • Chevalier, J.
  • Rocha, V. G.
  • Peijs, Ton
  • Reece, M. J.
  • Delia, E.
  • Reale, F.
  • Amit, I.
  • Palczynski, P.
  • Sherrell, Pc
  • Agnoli, S.
  • Craciun, Mf
  • Jones, Gf
  • Mehew, Jd
  • Mattevi, C.
  • Russo, S.
  • Bacon, A.
  • Sykes, J.
  • Grovenor, C.
  • Jenkins, M.
  • Lozano-Perez, S.
  • English, C.
  • Smith, G.
  • Yardley, S.
  • Lyon, S.
  • Preuss, M.
  • Moore, K.
  • Wei, J.
  • Wang, P.
  • Cottis, R.
  • Hudson, D.
  • Storer, S.
  • Chong, K.
  • Polatidis, E.
  • Fitzpatrick, M.
  • Comstock, R.
  • Ambard, A.
  • Blat-Yrieix, M.
  • Frankel, P.
  • Cottis, B.
  • Smith, J.
  • Hallstadius, L.
  • Saxey, D.
  • Hughes, G.
  • Terachi, T.
  • Yamada, T.
  • Kruska, K.
  • Mccomb, D.
  • Nicholls, R.
  • Nellist, P.
  • London, A.
  • Yates, Jr
  • Pickard, C.
  • Moat, R.
  • Forsey, A.
  • Frankel, P. G.
  • Comstock, R. J.
  • Preuss, Michael
  • Cottis, R. A.
  • Grovenor, Crm
  • Francis, E. M.
  • Grovenor, C. R. M.
  • Moat, Richard J.
  • Moore, Kl
  • Lyon, Stuart B.
  • Wei, J. F.
  • Yardley, S. S.
  • Moore, K. L.
  • Francis, E.
  • Smith, G. D. W.
  • Sykes, J. M.
  • Frankel, Philipp
  • Comstock, B.
  • Chong, K. B.
  • Fitzpatrick, M. E.
OrganizationsLocationPeople

document

Mechanisms of oxidation of fuel cladding alloys revealed by high resolution APT, TEM and SIMS analysis

  • Sykes, J. M.
  • Hudson, D.
  • Ni, N.
  • Grovenor, C. R. M.
  • Moore, Kl
  • Smith, G. D. W.
  • Lozano-Perez, S.
  • Yardley, S. S.
Abstract

Aqueous corrosion of zirconium alloys has become the major factor limiting prolonged fuel campaigns in nuclear plant. Studies using SEM, TEM and electrochemical impedance measurements have been interpreted as showing a dense inner-most oxide layer, and an increased thickness of the layer has been correlated to a better corrosion resistance. Many authors have reported that an 'intermediate layer' at the metal oxide interface has a complex structure or/and stochiometry different to that of both the bulk oxide and bulk metal, sometimes claimed to be a suboxide phase. Diffraction evidence has suggested the presence of both cubic ZrO and rhombohedral Zr 3O phases, and compositional analysis has revealed similar variations in local oxygen stoichiometry. We have carried out a systematic investigation of the structure and chemistry of the metal/oxide interface in samples of commercial ZIRLO corroded for times up to 180 days. We have developed new experimental techniques for the study of these interfaces both by Electron Energy Loss Spectroscopy (EELS) analysis in the Transmission Electron Microscope (TEM) and by Atom Probe Tomography (APT), and exactly the same samples have been investigated by both techniques. Our results show the development of a clearly defined suboxide layer of stoichiometry close to ZrO, and the subsequent disappearance of this layer at the first of the characteristic 'breakaway' transitions in the oxidation kinetics. We can correlate this behaviour with changes in the structure of the oxide layer, and particularly the development of interconnected porosity that links the corroding interface with the aqueous environment. Using high resolution SIMS analysis of isotopically spiked samples we demonstrate the penetration of the oxidising species through these porous outer oxide layers. © 2012 Materials Research Society.

Topics
  • porous
  • compound
  • corrosion
  • phase
  • scanning electron microscopy
  • Oxygen
  • zirconium
  • zirconium alloy
  • transmission electron microscopy
  • porosity
  • electron energy loss spectroscopy
  • selective ion monitoring
  • atom probe tomography