| People | Locations | Statistics |
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| Naji, M. |
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| Motta, Antonella |
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| Aletan, Dirar |
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| Mohamed, Tarek |
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| Ertürk, Emre |
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| Taccardi, Nicola |
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| Kononenko, Denys |
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| Petrov, R. H. | Madrid |
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| Alshaaer, Mazen | Brussels |
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| Bih, L. |
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| Casati, R. |
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| Muller, Hermance |
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| Kočí, Jan | Prague |
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| Šuljagić, Marija |
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| Kalteremidou, Kalliopi-Artemi | Brussels |
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| Azam, Siraj |
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| Ospanova, Alyiya |
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| Blanpain, Bart |
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| Ali, M. A. |
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| Popa, V. |
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| Rančić, M. |
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| Ollier, Nadège |
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| Azevedo, Nuno Monteiro |
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| Landes, Michael |
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| Rignanese, Gian-Marco |
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Ali, Abid
in Cooperation with on an Cooperation-Score of 37%
Topics
Publications (7/7 displayed)
- 2023Ecofriendly green synthesis of Ag@Cu bimetallic nanoparticles using <i>Seidlitzia stocksii</i> stem extract: photocatalytic degradation of methylene bluecitations
- 2023Surface engineered mesoporous silica carriers for the controlled delivery of anticancer drug 5-fluorouracil: Computational approach for the drug-carrier interactions using density functional theorycitations
- 2023Photocatalytic degradation of atrazine and abamectin using <i>Chenopodium album</i> leaves extract mediated copper oxide nanoparticlescitations
- 2022Heparin-Loaded Alginate Hydrogels: Characterization and Molecular Mechanisms of Their Angiogenic and Anti-Microbial Potentialcitations
- 2022Synthesis of poly (N-isopropyl acrylamide-co-2-acrylamido methylpropane sulfonic acid) hydrogel containing copper and nickel nanoparticles with easy recycling and efficient catalytic potentialcitations
- 2020Experimental Study on the Structural Behavior of Cast in-situ Hollow Core Concrete Slabscitations
- 2018Self-Sustaining Square-Extensional Mode Resonator Oscillator for Mass Sensing in Liquidcitations
Places of action
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article
Synthesis of poly (N-isopropyl acrylamide-co-2-acrylamido methylpropane sulfonic acid) hydrogel containing copper and nickel nanoparticles with easy recycling and efficient catalytic potential
Abstract
<jats:title>Abstract</jats:title><jats:p>Poly(N-isopropyl acrylamide-co-2-acrylamido methyl propane sulfonic acid) hydrogel was prepared and used as matrix for the fabrication of nickel and copper nanoparticles. Nickel and copper nanoparticles were fabricated via <jats:italic>in situ</jats:italic> reduction of Ni (II) and Cu (II) ions within the hydrogel matrix. The manufactured hydrogel and its corresponding composites with Ni and Cu nanoparticles were characterized by FTIR, XRD, EDX, TEM, and TGA. Thermal stability of hydrogel was found to be increased upon fabricating with metal nanoparticles. The hydrogel showed ability to absorb water 63 times of its weight in dried form. The Ni and Cu nanoparticles were observed to be well dispersed, spherical in shape and most of them were having diameters in the range of 12.5 to 38.8 nm and 58 to 102 nm, respectively. The as-prepared hydrogel-nickel and hydrogel-Cu nanocomposite were used as catalysts for the reduction of a toxic pollutant 4-nitrophenol. At 25 °C, the reduction of 4-NP was found to proceed with apparent rate constant (<jats:italic>k</jats:italic><jats:sub>app</jats:sub>) of 0.107 and 0.122 min<jats:sup>−1</jats:sup> in the presence of composite containing Ni and Cu nanoparticles, respectively. However, <jats:italic>k</jats:italic><jats:sub>app</jats:sub> was increased with corresponding increase in temperature and its maximum value was found to be 0.815 min<jats:sup>−1</jats:sup> at 88 °C with catalyst containing Ni nanoparticles. The formation of well dispersed Ni and Cu nanoparticles in the prepared hydrogel reflected that this hydrogel system can act as efficient stabilizing agent along with acting as a reactor medium. Recycling potential of catalysts was studied for five successive cycles.</jats:p>