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Naji, M. |
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Motta, Antonella |
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Aletan, Dirar |
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Mohamed, Tarek |
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Ertürk, Emre |
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Taccardi, Nicola |
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Kononenko, Denys |
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Petrov, R. H. | Madrid |
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Alshaaer, Mazen | Brussels |
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Bih, L. |
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Casati, R. |
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Muller, Hermance |
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Kočí, Jan | Prague |
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Šuljagić, Marija |
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Kalteremidou, Kalliopi-Artemi | Brussels |
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Azam, Siraj |
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Ospanova, Alyiya |
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Blanpain, Bart |
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Ali, M. A. |
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Popa, V. |
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Rančić, M. |
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Ollier, Nadège |
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Azevedo, Nuno Monteiro |
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Landes, Michael |
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Rignanese, Gian-Marco |
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Heymann, Gunter
Universität Innsbruck
in Cooperation with on an Cooperation-Score of 37%
Topics
Publications (9/9 displayed)
- 2023Tb2Co(B2O5)2 and Tb2Cu(B2O5)2 – two new borates with gadolinite-type structurescitations
- 2023Crystal structures and luminescence properties of Li6MN4:Ce3+ (M = Mo, W)
- 2019Serendipitous formation and characterization of K2[Pd(NO3)4]·2HNO3
- 2018Synthesis and characterization of the new tin borate SnB8O11(OH)4citations
- 2017The high-pressure phase of CePtAlcitations
- 2016Synthesis and characterization of the novel rare earth orthophosphates Y0.5Er0.5PO4 and Y0.5Yb0.5PO4citations
- 2016Hydrothermal synthesis of a new lead(II) borate (Pb4O)Pb2B6O14-IIcitations
- 2013Ce4Ag3Ge4O0.5 - chains of oxygen-centered OCe2Ce2/2] tetrahedra embedded in a CeAg3Ge4] intermetallic matrixcitations
- 2005High-Pressure Synthesis of a Gallium Oxonitride with a Spinel-Type Structurecitations
Places of action
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article
High-Pressure Synthesis of a Gallium Oxonitride with a Spinel-Type Structure
Abstract
<jats:p>The new compound Ga<jats:sub>2.81</jats:sub>O<jats:sub>3.57</jats:sub>N<jats:sub>0.43</jats:sub> was crystallized under high-pressure / high-temperature conditions in a spinel-type structure from a prestructured gallium oxonitride ceramic, which was obtained from the single-source molecular precursor [Ga(O<jats:sup>t</jats:sup>Bu)<jats:sub>2</jats:sub>NMe<jats:sub>2</jats:sub>]<jats:sub>2</jats:sub> by thermal treatment in an ammonia atmosphere. The optimized precursor-derived gallium oxonitride ceramic remains nanocrystalline up to 600 °C and can be transformed at 7 GPa and 1100 °C into the crystalline phase Ga<jats:sub>2.81</jats:sub>O<jats:sub>3.57</jats:sub>N<jats:sub>0.43</jats:sub>. The structure, homogeneity, and nitrogen to oxygen ratio were determined using TEM coupled with an electron energy loss spectrometer (EELS) and an energy dispersive X-ray (EDX) spectrometer. For phase analysis and structure confirmation, X-ray powder diffraction data were measured.</jats:p>