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Naji, M. |
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Motta, Antonella |
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Aletan, Dirar |
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Mohamed, Tarek |
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Ertürk, Emre |
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Taccardi, Nicola |
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Kononenko, Denys |
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Petrov, R. H. | Madrid |
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Alshaaer, Mazen | Brussels |
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Bih, L. |
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Casati, R. |
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Muller, Hermance |
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Kočí, Jan | Prague |
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Šuljagić, Marija |
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Kalteremidou, Kalliopi-Artemi | Brussels |
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Azam, Siraj |
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Ospanova, Alyiya |
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Blanpain, Bart |
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Ali, M. A. |
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Popa, V. |
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Rančić, M. |
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Ollier, Nadège |
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Azevedo, Nuno Monteiro |
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Landes, Michael |
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Rignanese, Gian-Marco |
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Seide, Gunnar
in Cooperation with on an Cooperation-Score of 37%
Topics
Publications (11/11 displayed)
- 2024Synthesis, mechanical characterisation and modeling of super flexible silica aerogels and their joining techniques
- 2022Curcumin and Silver Doping Enhance the Spinnability and Antibacterial Activity of Melt-Electrospun Polybutylene Succinate Fiberscitations
- 2022Pilot-Scale Electrospinning of PLA Using Biobased Dyes as Multifunctional Additivescitations
- 2020The effect of additives and process parameters on the pilot-scale manufacturing of polylactic acid sub-microfibers by melt electrospinningcitations
- 2020The Effect of Dye and Pigment Concentrations on the Diameter of Melt-Electrospun Polylactic Acid Fiberscitations
- 2020Pilot-scale production of polylactic acid nanofibers by melt electrospinningcitations
- 2019Novel Bicomponent Functional Fibers with Sheath/Core Configuration Containing Intumescent Flame-Retardants for Textile Applicationscitations
- 2019Pilot-scale fabrication and analysis of graphene-nanocomposite fiberscitations
- 2019The Efficiency of Biobased Carbonization Agent and Intumescent Flame Retardant on Flame Retardancy of Biopolymer Composites and Investigation of their Melt-Spinnabilitycitations
- 2019From Lab to Pilot Scale: Melt Electrospun Nanofibers of Polypropylene with Conductive Additives
- 2019Investigation of the Flammability and Thermal Stability of Halogen-Free Intumescent System in Biopolymer Composites Containing Biobased Carbonization Agent and Mechanism of Their Char Formationcitations
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article
Pilot-scale production of polylactic acid nanofibers by melt electrospinning
Abstract
Melt electrospinning has been used to manufacture fibers with diameters in the low micrometer range, but the production of submicrometer fibers has proven more challenging. In this study, we investigated the feasibility of fabricating polylactic acid nanofibers using polymer grades with the increasing melt flow rates (15–85 g/10 min at 210°C) by melt electrospinning with a 600-nozzle pilot-scale device featuring an integrated climate control system realized as a glass chamber around the spinneret. Previous experiments using this device without appropriate climate control produced fibers exceeding 1µm in diameter because the drawing of fibers was inhibited by the rapid cooling of the polymer melt. The integrated glass chamber created a temperature gradient exceeding the glass transition temperature of the polymer, which enhanced the drawing of fibers below the spinneret. An average fiber diameter of 810 nm was achieved using Ingeo Biopolymer 6252, and the finest individual fiber (420 nm in diameter) was produced at a spin pump speed of 5 rpm and a spinneret set temperature of 230°C. We have therefore demonstrated the innovative performance of our pilot-scale melt-electrospinning device, which bridges the gap between laboratory-scale and pilot-scale manufacturing and achieves fiber diameters comparable to those produced by conventional solution electrospinning.<br/>