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Molga, Eugeniusz
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article
Pyrolysis of waste tyres – The effect of reaction kinetics on the results of thermogravimetric analysis
Abstract
Thispaperpresentsasystematicthermogravimetric(TG)studyonthekineticsofend-of-lifetyre(ELT) pyrolysis. In the experimental part of this work, TG results are compared for tyre samples ofdifferentmassandsize.Thisshowsthattheconductionresistanceinthemilligramscale(upto~100 mg) tyre sample can be neglected. A comparison of experimental results demonstrates that thecharacteristicmaximaontheDTGcurve(thefirstderivativeofTGsignal)shifttowardshighertemperatures for higher heating rates. This phenomenon is explained to have kinetic origin and it isnotcausedbytheinternalheattransferresistance.Inthemodellingpartofthiswork,thekineticparameters of the Three-Component Simulation Model (TCSM) are calculated and compared to theliteraturevalues.Testingofthekineticmodeliscarriedoutusingexperimentswithavaryingheatingrate.Thisshowsthelimitationofthesimplifiedkineticapproachandtheappropriateselection method of the kinetic parameters.