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Naji, M. |
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Motta, Antonella |
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Aletan, Dirar |
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Mohamed, Tarek |
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Ertürk, Emre |
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Taccardi, Nicola |
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Kononenko, Denys |
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Petrov, R. H. | Madrid |
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Alshaaer, Mazen | Brussels |
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Bih, L. |
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Casati, R. |
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Muller, Hermance |
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Kočí, Jan | Prague |
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Šuljagić, Marija |
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Kalteremidou, Kalliopi-Artemi | Brussels |
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Azam, Siraj |
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Ospanova, Alyiya |
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Blanpain, Bart |
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Ali, M. A. |
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Popa, V. |
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Rančić, M. |
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Ollier, Nadège |
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Azevedo, Nuno Monteiro |
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Landes, Michael |
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Rignanese, Gian-Marco |
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Andersen, Shuang Ma
in Cooperation with on an Cooperation-Score of 37%
Topics
Publications (30/30 displayed)
- 2022Post-degradation case study of the membrane electrode assembly from a low-temperature PEMFC stack
- 2022Post-degradation case study of the membrane electrode assembly from a low-temperature PEMFC stack
- 2022Microwave-Assisted Scalable Synthesis of Pt/Ccitations
- 2022Microwave-Assisted Scalable Synthesis of Pt/C:Impact of the Microwave Irradiation and Carrier Solution Polarity on Nanoparticle Formation and Aging of the Support Carboncitations
- 2022Insights into Degradation of the Membrane–Electrode Assembly Performance in Low-Temperature PEMFC:the Catalyst, the Ionomer, or the Interface?citations
- 2022Towering non-Faradaic capacitive storage based on high quality reduced graphene oxide from spent graphitecitations
- 2022Insights into Degradation of the Membrane–Electrode Assembly Performance in Low-Temperature PEMFCcitations
- 2021Degradation mechanisms of electrochemical activity of Pt/C during the accelerated stress test focused on catalyst support corrosion
- 2020Preparation and Characterization of Poly(Vinyl Alcohol) (PVA)/SiO 2 , PVA/Sulfosuccinic Acid (SSA) and PVA/SiO 2 /SSA Membranes:A Comparative Studycitations
- 2020Solution combustion synthesized ceria or alumina supported Pt as cathode electrocatalyst for PEM fuel cellscitations
- 2020Preparation and Characterization of Poly(Vinyl Alcohol) (PVA)/SiO2, PVA/Sulfosuccinic Acid (SSA) and PVA/SiO2/SSA Membranescitations
- 2020Platinum recycling through electroless dissolution under mild conditions using a surface activation assisted Pt-complexing approachcitations
- 2020Platinum recycling through electroless dissolution under mild conditions using a surface activation assisted Pt-complexing approachcitations
- 2019Influence of dispersion media on Nafion® ionomer distribution in proton exchange membrane fuel cell catalyst carbon supportcitations
- 2019Influence of dispersion media on Nafion® ionomer distribution in proton exchange membrane fuel cell catalyst carbon supportcitations
- 2018Accurate Determination of Catalyst Loading on Glassy Carbon Disk and Its Impact on Thin Film Rotating Disk Electrode for Oxygen Reduction Reactioncitations
- 2018Exploring the XRF technique as a tool to estimate the degree of leaching in alloy-catalysts used for PEMFCs
- 2018Environmentally and industrially friendly recycling of platinum nanoparticles through electrochemical dissolution–electrodeposition in acid‐free/dilute acidic electrolytescitations
- 2018Environmentally and industrially friendly recycling of platinum nanoparticles through electrochemical dissolution–electrodeposition in acid‐free/dilute acidic electrolytescitations
- 2018Accurate determination of catalyst loading on glassy carbon disk and its impact on thin film rotating disk electrode for oxygen reduction reaction.
- 2018Investigating the single-step solution combustion method for synthesis of oxide supported/unsupported Pt/PtOx, as cathode electrocatalysts for PEMFCs
- 2017Helium Ion Microscopy of proton exchange membrane fuel cell electrode structurescitations
- 2017Helium Ion Microscopy of proton exchange membrane fuel cell electrode structurescitations
- 2016Nano carbon supported platinum catalyst interaction behavior with perfluorosulfonic acid ionomer and their interface structurescitations
- 2015Tin Dioxide as an Effective Antioxidant for Proton Exchange Membrane Fuel Cellscitations
- 2015Tin Dioxide as an Effective Antioxidant for Proton Exchange Membrane Fuel Cellscitations
- 2014Influence of different carbon nanostructures on the electrocatalytic activity and stability of Pt supported electrocatalystscitations
- 2014Influence of different carbon nanostructures on the electrocatalytic activity and stability of Pt supported electrocatalystscitations
- 2013Durability of Carbon Nanofiber (CNF) & Carbon Nanotube (CNT) as Catalyst Support for Proton Exchange Membrane Fuel Cellscitations
- 2012Interaction between Nafion ionomer and noble metal catalyst for PEMFCs
Places of action
Organizations | Location | People |
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document
Accurate determination of catalyst loading on glassy carbon disk and its impact on thin film rotating disk electrode for oxygen reduction reaction.
Abstract
Thin film-rotating disc electrode (TF- RDE) experiment provides a fast research platform for screening of newly developed electrocatalysts for oxygen reduction reaction (ORR) activity, however, precise estimation of their performance parameters is necessary to avoid wastage of resources in the testing of otherwise unpromising electrocatalyst in actual fuel cells. Here the importance of accurate amount of catalyst (e.g. Pt) on GC disk of RDE in TF-RDE experiment is presented by characterizing the inks based on commercial catalysts for their electrocatalysis performance (ORR activity) and while estimating the performance parameters. The amount Pt loadings estimated using literature based (conventional) scheme as well as, the proposed, X-ray fluorescent (XRF) based scheme is presented. A parameter defined as ‘catalyst-density-of-the-ink’, which is based on estimated Pt-loadings using conventional and XRF based scheme, is used to correlate the variation observed in the estimated performance values and the amount of Pt on GC disk of RDE. The investigation suggests that the actual Pt loading on GC disk of RDE varies with the ink-conditions, which is considered constant in the conventional scheme, might be leading to irreproducibility of the data obtained by TF-RDE experiments. The XRF based scheme, which is simple and direct, can have the potential to replace conventional scheme for accurate catalyst loading estimation, improve experimental reproducibility and open many other possibilities (e.g. catalyst loading determination after tests) in electrocatalysis studies.