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Naji, M. |
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Motta, Antonella |
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Aletan, Dirar |
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Mohamed, Tarek |
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Ertürk, Emre |
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Taccardi, Nicola |
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Kononenko, Denys |
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Petrov, R. H. | Madrid |
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Alshaaer, Mazen | Brussels |
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Bih, L. |
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Casati, R. |
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Muller, Hermance |
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Kočí, Jan | Prague |
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Šuljagić, Marija |
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Kalteremidou, Kalliopi-Artemi | Brussels |
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Azam, Siraj |
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Ospanova, Alyiya |
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Blanpain, Bart |
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Ali, M. A. |
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Popa, V. |
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Rančić, M. |
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Ollier, Nadège |
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Azevedo, Nuno Monteiro |
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Landes, Michael |
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Rignanese, Gian-Marco |
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Azevedo, J.
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Publications (7/7 displayed)
- 2018High purity and crystalline thin films of methylammonium lead iodide perovskites by a vapor deposition approachcitations
- 2017On the Deposition of Lead Halide Perovskite Precursors by Physical Vapor Methodcitations
- 2016Soluble Salts Amplify the Effect of Small Heterogeneities in the Structure of Porous Building Materials During Dryingcitations
- 2016Friction Stir Welding of Shipbuilding Steel with Primercitations
- 2014Ultra-long Fe nanowires by pulsed electrodeposition with full filling of alumina templatescitations
- 2012Influence of the Rest Pulse Duration in Pulsed Electrodeposition of Fe Nanowirescitations
- 2011Serum total and bone alkaline phosphatase and tartrate-resistant acid phosphatase activities for the assessment of bone fracture healing in dogscitations
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article
Influence of the Rest Pulse Duration in Pulsed Electrodeposition of Fe Nanowires
Abstract
Highly uniform iron nanowires were synthesized in porous anodic alumina, through a pulsed electrodeposition method. The effect of the rest pulse duration in the deposition quality was systematically investigated, being the best duration found at 0.6 s with 91.9% of pores filled. A methodology of surface response design of experiment was conducted to find the optimum predicted value for the rest pulse duration, by controlling the following experimental parameters/variables: current density, electrolyte concentration and temperature. The influence of the rest pulse in the grain size of the iron nanowires was also studied trough X-ray diffraction patterns. A numerical simulation of the concentration evolution along a nanopore was performed, allowing to achieve a deeper understanding of the importance of the rest pulse in the NW electrodeposition.