Materials Map

Discover the materials research landscape. Find experts, partners, networks.

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The Materials Map is an open tool for improving networking and interdisciplinary exchange within materials research. It enables cross-database search for cooperation and network partners and discovering of the research landscape.

The dashboard provides detailed information about the selected scientist, e.g. publications. The dashboard can be filtered and shows the relationship to co-authors in different diagrams. In addition, a link is provided to find contact information.

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Materials Map under construction

The Materials Map is still under development. In its current state, it is only based on one single data source and, thus, incomplete and contains duplicates. We are working on incorporating new open data sources like ORCID to improve the quality and the timeliness of our data. We will update Materials Map as soon as possible and kindly ask for your patience.

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Haigh, Sj

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University of Manchester

in Cooperation with on an Cooperation-Score of 37%

Topics

Publications (63/63 displayed)

  • 2024Electron beam and thermal stabilities of MFM-300(M) metal–organic frameworks †2citations
  • 2024Understanding Ag liquid migration in SiC through ex-situ and in-situ Ag-Pd/SiC interaction studies2citations
  • 2024Electron Beam and Thermal Stabilities of MFM-300(M) Metal-Organic Frameworks2citations
  • 2023A Low‐Temperature Synthetic Route Toward a High‐Entropy 2D Hexernary Transition Metal Dichalcogenide for Hydrogen Evolution Electrocatalysis39citations
  • 2023Copper bioreduction and nanoparticle synthesis by an enrichment culture from a former copper mine3citations
  • 2023A high-resolution versatile focused ion implantation platform for nanoscale engineering5citations
  • 2023Exfoliablity, magnetism, energy storage and stability of metal thiophosphate nanosheets made in liquid medium.12citations
  • 2022Hydrotalcite colloid stability and interactions with uranium(VI) at neutral to alkaline pH.16citations
  • 2021High Performance Nanostructured MoS2 Electrodes with Spontaneous Ultra-Low Gold Loading for Hydrogen Evolution15citations
  • 2021Synthesis of molybdenum-doped rhenium disulfide alloy using aerosol-assisted chemical vapour deposition9citations
  • 2020Comparing Xe+pFIB and Ga+FIB for TEM sample preparation of Al alloys: Minimising FIB-induced artefacts52citations
  • 2020Capillary condensation under atomic-scale confinement254citations
  • 2020Atomic Resolution Imaging of CrBr3 using Adhesion-Enhanced Grids17citations
  • 2020Splenic Capture and In Vivo Intracellular Biodegradation of Biological-grade Graphene Oxide Sheets71citations
  • 2020Large magnetoelectric coupling in multiferroic oxide heterostructures assembled via epitaxial lift-off.citations
  • 2019Imaging three-dimensional elemental inhomogeneity in Pt–Ni nanoparticles using spectroscopic single particle reconstruction26citations
  • 2019Formation and healing of defects in atomically thin GaSe and InSe48citations
  • 2019Chemical vapor deposition of tin sulfide from diorganotin(IV) dixanthates27citations
  • 2019Indirect to direct gap crossover in two-dimensional InSe revealed by angle-resolved photoemission spectroscopy104citations
  • 2018Atomic-Scale Insights into the Oxidation of Aluminum118citations
  • 2018Infrared-to-violet tunable optical activity in atomic films of GaSe, InSe, and their heterostructures65citations
  • 2018Nanometer Resolution Elemental Mapping in Graphene-based TEM Liquid Cells124citations
  • 2018Anomalous twin boundaries in two dimensional materials62citations
  • 2018Biosynthesis and Characterization of Copper Nanoparticles Using Shewanella oneidensis: Application for Click Chemistry139citations
  • 2017A Single Source Precursor for Tungsten Dichalcogenide Thin Films: Mo1-xWxS2 (0 ≤ x ≤ 1) Alloys by Aerosol-Assisted Chemical Vapor Deposition (AACVD)32citations
  • 2017Enhanced organophilic separations with mixed matrix membranes of polymers of intrinsic microporosity and graphene-like fillers58citations
  • 2017In Situ Industrial Bimetallic Catalyst Characterisation using Scanning Transmission Electron Microscopy and X-Ray Absorption Spectroscopy at One Atmosphere and Elevated Temperature17citations
  • 2017Observing imperfection in atomic interfaces for van der Waals heterostructures77citations
  • 2017Solution Processing of Two-Dimensional Black Phosphorus67citations
  • 2017EXPLORING NANOSCALE PRECURSOR REACTIONS IN ALLOY 600 IN H2/N2-H2O VAPOR USING IN SITU ANALYTICAL TRANSMISSION ELECTRON MICROSCOPY1citations
  • 2017Analysis of grain size in FePt films fabricated using remote plasma depositioncitations
  • 2017Mapping grain boundary heterogeneity at the nanoscale in a positive temperature coefficient of resistivity ceramic16citations
  • 2017Magnetoresistance of vertical Co-graphene-NiFe junctions controlled by charge transfer and proximity-induced spin splitting in graphene97citations
  • 2017Multiscale correlative tomography: an investigation of creep cavitation in 316 stainless steel44citations
  • 2017Role of 2D and 3D defects on the reduction of LaNiO3 nanoparticles for catalysis32citations
  • 2016Recent progress in scanning transmission electron microscope imaging and analysis1citations
  • 2016An investigation of diffusion-mediated cyclic coarsening and reversal coarsening in an advanced Ni-based superalloy82citations
  • 2016Metal-organic framework templated electrodeposition of functional gold nanostructures53citations
  • 2016Asymmetric MoS2-graphene-metal sandwiches: Preparation, characterization and application74citations
  • 2016The Application of In Situ Analytical Transmission Electron Microscopy to the Study of Preferential Intergranular Oxidation in Alloy 60041citations
  • 2016Imaging the hydrated microbe-metal interface using nanoscale spectrum imaging2citations
  • 2016Radiation damage in biotite mica by accelerated α-particles: A synchrotron microfocus X-ray diffraction and X-ray absorption spectroscopy study7citations
  • 2016Dislocation core structures in (0001) InGaN19citations
  • 2016Synthesis and characterization of composite membranes made of graphene and polymers of intrinsic microporosity34citations
  • 2015Compositional variations for small-scale gamma prime (γ′) precipitates formed at different cooling rates in an advanced Ni-based superalloy93citations
  • 2015Grain Boundary Segregation of Rare-Earth Elements in Magnesium Alloys126citations
  • 2015Preparation of low-dimensional carbon material-based metal nanocomposites using a polarisable organic/water interface11citations
  • 2015Behavior of alloying elements during anodizing of Mg-Cu and Mg-W alloys in a fluoride/glycerol electrolyte6citations
  • 2015Synthesis of Lateral Size-Controlled Monolayer 1H-MoS2@Oleylamine as Supercapacitor Electrodes.142citations
  • 2015In Situ Synthesis of PbS Nanocrystals in Polymer Thin Films from Lead(II) Xanthate and Dithiocarbamate Complexes: Evidence for Size and Morphology Control88citations
  • 2014On the diffusion mechanisms of fine-scale γ ′ in an advanced Ni-based superalloy1citations
  • 2014Real-time imaging and elemental mapping of AgAu nanoparticle transformations65citations
  • 2014Correlative tomography145citations
  • 2014Understanding the limitations of the Super-X energy dispersive x-ray spectrometer as a function of specimen tilt angle for tomographic data acquisition in the S/TEM21citations
  • 2014Kink Band Formation in Graphite under Ion Irradiation at 100 and 298K9citations
  • 2014Formation of barrier-type anodic films on ZE41 magnesium alloy in a fluoride/glycerol electrolyte27citations
  • 2013Reversible loss of bernal stacking during the deformation of few-layer graphene in nanocomposites74citations
  • 2012Direct measurement of the crystallographically sensitive atomic termination of nanophase cerium dioxidecitations
  • 2012Exit wave reconstruction from focal series of HRTEM images, single crystal XRD and total energy studies on Sb xWO 3+y (x ~ 0.11)8citations
  • 2011New routes to copper sulfide nanostructures and thin films70citations
  • 2010Exceeding conventional resolution limits in high-resolution transmission electron microscopy using tilted illumination and exit-wave restoration7citations
  • 2005Chemical interactions in Ti doped MgB2 superconducting bulk samples and wires27citations
  • 2004Improvement of the current carrying capability of ex situ MgB2 wires by normal particle additions45citations

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Prikhna, T. A.
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Kovac, P.
1 / 5 shared
Kilburn, M. R.
1 / 3 shared
Savchuk, Ya M.
1 / 1 shared
Salter, C.
1 / 7 shared
Hutchison, J.
1 / 9 shared
Melişek, T.
1 / 1 shared
Grovenor, C. R. M.
1 / 18 shared
Kováč, P.
1 / 1 shared
Hušek, I.
1 / 1 shared
Jones, H.
1 / 21 shared
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  • Allen, Cs
  • Tien, E.
  • Carter, Jh
  • Cao, G.
  • Ngo, D.
  • Schröder, M.
  • Tang, Cc
  • Yang, S.
  • Tillotson, E.
  • Thompson, Sp
  • Clark, N.
  • Chen, Y.
  • Liu, Xuzhao
  • Lindley, Matthew
  • Withers, Pj
  • Cao, Huatang
  • Shepherd, Daniel
  • Su, Zixian
  • Zhong, Xiangli
  • Wei, Kerui
  • Donoghue, Jack
  • Xiao, Ping
  • Eggeman, Alexander
  • Martins, João P.
  • Kho, Zhiquan
  • Liu, Han
  • Tien, Eu Pin
  • Tang, Chiu
  • Yang, Sihai
  • Chen, Yinlin
  • Schroder, Martin
  • Carter, Joseph
  • Tillotson, Evan
  • Cao, Guanhai
  • Thompson, Stephen
  • Allen, Christopher
  • Ngo, Duc-The
  • Clark, Nick
  • Latour, Hugo De
  • Walton, Alex
  • Whitehead, George F. S.
  • Smith, Charles T.
  • Hazeldine, Kerry
  • Skelton, Jonathan M.
  • Qu, Jie
  • Buckingham, Mark A.
  • Elgendy, Amr
  • Papaderakis, Athanasios A.
  • Binks, Dj
  • Lewis, Dj
  • Cai, Rongsheng
  • Alam, Firoz
  • Lloyd, Jonathan R.
  • Jedyka, Klaudia
  • Boothman, Christopher
  • Kimber, Richard
  • Elizondo, Gretta
  • Bagshaw, Heath
  • Coker, Victoria S.
  • Curry, Rj
  • Lagator, Matija
  • Moore, Kl
  • Li, Kexue
  • Adshead, Mason
  • Almutawa, Abdulwahab
  • Lockyer, Nicholas P.
  • Bellew, Allen
  • Gourlay, Cm
  • Aresta, Gianfranco
  • Coke, Maddison
  • Cui, Yi
  • Bensch, Wolfgang
  • Mccrystall, Mark
  • Wurstbauer, Ursula
  • Konkena, Bharathi
  • Saigal, Nihit
  • Spillecke, Lena
  • Konečný, Jan
  • Tiede, David
  • Dinter, Jonas Van
  • Klingeler, Rüdiger
  • Müller, Alina
  • Sofer, Zdenek
  • Kelly, Daniel
  • Shao, Shouqi
  • Synnatschke, Kevin
  • Coleman, Jonathan
  • Backes, Claudia
  • Harrison, Robert W.
  • Neill, Thomas
  • Sherriff, Nick
  • Wilson, Hannah
  • Odriozola, Laura Lopez
  • Shaw, Samuel
  • Natrajan, Louise
  • Foster, Chris
  • Bryan, Nick
  • Morris, Katherine
  • Rigby, Bruce
  • Zou, Yi Chao
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  • Higgins, Eliott
  • Byrne, Conor
  • Papaderakis, Athanasios
  • Mcnaughter, Paul D.
  • Al-Shakban, Mundher
  • Lewis, Edward A.
  • Al-Dulaimi, Naktal
  • Wade, C. Austin
  • Cai, Changrun
  • Zhou, Xiaorong
  • Yang, Qian
  • Geim, Andre
  • Wang, F. C.
  • Grigorieva, Irina
  • Zhou, Zuowan
  • Fumagalli, Laura
  • Stebunov, Yury
  • Sun, Pengzhan
  • Zou, Yichao
  • Hopkinson, David G.
  • Wang, Wendong
  • Gorbachev, Roman V.
  • Bointon, Thomas H.
  • Hamer, Matthew J.
  • Kelly, Daniel J.
  • Zhou, Mingwei
  • Assas, Mushref
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  • Rey, Irene De Lazaro Del
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  • Newman, Leon
  • Lozano, Neus
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  • Prestat, Eric
  • Bussy, Cyrill
  • Farokhipoor, S.
  • Ghidini, M.
  • Khestanova, E.
  • Dhesi, Ss
  • Mathur, Nd
  • Zhang, S.
  • Kim, J.
  • Pesquera, D.
  • Rooney, Ap
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  • Vickers, Me
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  • Moya, X.
  • Young, Neil P.
  • Leteba, Gerard M.
  • Race, Christopher P.
  • Slater, Thomas J. A.
  • Wang, Yi-Chi
  • Kirkland, Angus I.
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  • Lang, Candace I.
  • Terry, Dj
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  • Falko, Vladimir I.
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  • Patanè, Amalia
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  • Matthews, Peter D.
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  • Graham, Abigail J.
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  • Terry, Daniel
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  • Burnett, Tl
  • Zakharov, Dmitri N.
  • Thompson, George
  • Stach, Eric A.
  • Berkels, Benjamin
  • Nguyen, Lan
  • Rakowski, Alexander M.
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  • Terry, Daniel J.
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  • Young, Robert J.
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  • Budd, Peter M.
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  • Gregg, Jm
  • Ramasse, Quentin M.
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  • Kumar, Amit
  • Ward, Michael B.
  • Douglas, Am
  • Holsgrove, Kristina M.
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  • Hill, Ernie
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  • Laurie, Helen
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  • Humphreys, C. J.
  • Mcaleese, C.
  • Pennycook, T. J.
  • Rhode, S. L.
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  • Malik, Azad
  • Francis, E. M.
  • Slater, T. J. A.
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  • Lewis, E. A.
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  • Janus, M.
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  • Young, N. P.
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  • Grovenor, C.
  • Prikhna, T. A.
  • Kovac, P.
  • Kilburn, M. R.
  • Savchuk, Ya M.
  • Salter, C.
  • Hutchison, J.
  • Melişek, T.
  • Grovenor, C. R. M.
  • Kováč, P.
  • Hušek, I.
  • Jones, H.
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article

Comparing Xe+pFIB and Ga+FIB for TEM sample preparation of Al alloys: Minimising FIB-induced artefacts

  • Haigh, Sj
  • Zhong, Xiangli
  • Wade, C. Austin
  • Cai, Changrun
  • Withers, Pj
  • Zhou, Xiaorong
Abstract

Recently, the dual beam Xe+ plasma focused ion beam (Xe+pFIB) instrument has attracted increasing interest for site‐specific transmission electron microscopy (TEM) sample preparation for a local region of interest as it shows several potential benefits compared to conventional Ga+FIB milling. Nevertheless, challenges and questions remain especially in terms of FIB‐induced artefacts, which hinder reliable S/TEM microstructural and compositional analysis. Here we examine the efficacy of using Xe+ pFIB as compared with conventional Ga+ FIB for TEM sample preparation of Al alloys. Three potential source of specimen preparation artefacts were examined, namely: (1) implantation‐induced defects such as amophisation, dislocations, or ‘bubble’ formation in the near‐surface region resulting from ion bombardment of the sample by the incident beam; (2) compositional artefacts due to implantation of the source ions and (3) material redeposition due to the milling process. It is shown that Xe+pFIB milling is able to produce improved STEM/TEM samples compared to those produced by Ga+ milling, and is therefore the preferred specimen preparation route. Strategies for minimising the artefacts induced by Xe+pFIB and Ga+FIB are also proposed.<br/>Lay DescriptionFIB (focused ion beam) instruments have become one of the most important systems in the preparation of site‐specific TEM specimens, which are typically 50‐100 nm in thickness. TEM specimen preparation of Al alloys is particularly challenging, as convention Ga‐ion FIB produces artefacts in these materials that make microstructural analysis difficult or impossible. Recently, the use of noble gas ion sources, such as Xe, has markedly improved milling speeds and is being used for the preparation of various materials. Hence, it is necessary to investigate the structural defects formed during FIB milling and assess the ion‐induced chemical contamination in these TEM samples. Here we explore the feasibility and efficiency of using Xe+PFIB as a TEM sample preparation route for Al alloys in comparison with the conventional Ga+FIB.

Topics
  • impedance spectroscopy
  • surface
  • grinding
  • milling
  • focused ion beam
  • transmission electron microscopy
  • dislocation