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Naji, M. |
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Motta, Antonella |
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Aletan, Dirar |
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Mohamed, Tarek |
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Ertürk, Emre |
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Taccardi, Nicola |
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Kononenko, Denys |
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Petrov, R. H. | Madrid |
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Alshaaer, Mazen | Brussels |
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Bih, L. |
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Casati, R. |
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Muller, Hermance |
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Kočí, Jan | Prague |
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Šuljagić, Marija |
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Kalteremidou, Kalliopi-Artemi | Brussels |
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Azam, Siraj |
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Ospanova, Alyiya |
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Blanpain, Bart |
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Ali, M. A. |
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Popa, V. |
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Rančić, M. |
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Ollier, Nadège |
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Azevedo, Nuno Monteiro |
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Landes, Michael |
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Rignanese, Gian-Marco |
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Krawczyńska, Agnieszka
in Cooperation with on an Cooperation-Score of 37%
Topics
Publications (15/15 displayed)
- 2020In vitro evaluation of degradable electrospun polylactic acid/bioactive calcium phosphate ormoglass scaffoldscitations
- 20203D DIC-assisted residual stress measurement in 316 LVM steel processed by HE and HPTcitations
- 2019New approach to amorphization of alloys with low glass forming ability via selective laser meltingcitations
- 2019Mechanical properties and corrosion resistance of hydrostatically extruded 316 LVM stainless steel after low-temperature plasma nitridingcitations
- 2019Analysis of the microstructure of an AZ31/AA1050/AA2519 laminate produced using the explosive-welding methodcitations
- 2018Microstructural characterization and residual stress distribution in a nanostructured austenitic stainless steelcitations
- 2018Formation of the Nitrided Layers on an Austenitic Stainless Steel with Different Grain Structurescitations
- 2017New synthesis route to decorate Li 4 Ti 5 O 12 grains with GO flakescitations
- 2017Mechanical properties and corrosion resistance of ultrafine grained austenitic stainless steel processed by hydrostatic extrusioncitations
- 2017Microstructure and mechanical properties investigation of CP titanium processed by selective laser melting (SLM)citations
- 2017Analysis of microstructural aspects of a hip stem failure made of the REX 734 stainless steelcitations
- 2017The effect of current types on the microstructure and corrosion properties of Ni/NANOAl2O3 composite coatings
- 2016STEM study of Li4Ti5O12 anode material modified with Ag nanoparticlescitations
- 2014Strength of nanostructured austenitic steel 316LN at cryogenic temperaturescitations
- 2013Strain relaxation and grain growth in 316LVM stainless steel annealed under pressure
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article
STEM study of Li4Ti5O12 anode material modified with Ag nanoparticles
Abstract
Comprehensive scanning transmission electron microscopy(STEM) analysis of Li4Ti5O12 (LTO) powder modified by deposited Ag nanoparticles was performed. Nanocomposite powders with Ag content of 1 wt.%, 4 wt.%, 10 wt.% were fabricated in a chemical process from suspensions of Ag and LTO. Apart from the STEM results, the presence of pure silver on the surface of the ceramic powder was confirmed by XRD and XPS analyses. The silver particles deposited on the LTO particles were characterized using the EDS mapping technique. The quantified results of the EDS mapping showed a relatively homogenous distribution of silver nanoparticles on the powder surface for every metal content. The mean diameter of the nanoparticles deposited on the LTO powder was about 4 nm in all cases. An increase in the Ag content during chemical surfacemodification did not cause changes in themicrostructure. Focusing on an analysis of the metallic nanoparticles on the ceramic powder, electron tomography was used as an investigative technique. A very precise analysis of three dimensional nanostructures is desirable for a comprehensive analysis of complex materials. The quantified analysis of the Ag nanoparticles visualized using electron tomography confirmed the results of the size measurements taken from the two-dimensional EDS maps.