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Naji, M. |
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Motta, Antonella |
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Aletan, Dirar |
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Mohamed, Tarek |
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Ertürk, Emre |
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Taccardi, Nicola |
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Kononenko, Denys |
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Petrov, R. H. | Madrid |
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Alshaaer, Mazen | Brussels |
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Bih, L. |
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Casati, R. |
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Muller, Hermance |
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Kočí, Jan | Prague |
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Šuljagić, Marija |
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Kalteremidou, Kalliopi-Artemi | Brussels |
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Azam, Siraj |
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Ospanova, Alyiya |
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Blanpain, Bart |
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Ali, M. A. |
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Popa, V. |
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Rančić, M. |
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Ollier, Nadège |
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Azevedo, Nuno Monteiro |
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Landes, Michael |
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Rignanese, Gian-Marco |
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Roguska, Agata
Laboratoire Bourguignon des Matériaux et Procédés
in Cooperation with on an Cooperation-Score of 37%
Topics
Publications (9/9 displayed)
- 2023Coatings deposited by physical vapor deposition (PVD) on high-speed steel used in the processing of wood materials
- 2021Influence of microstructural features on the growth of nanotubular oxide layers on β-phase Ti-24Nb-4Zr-8Sn and α + β-phase Ti-13Nb-13Zr alloyscitations
- 2020In vitro evaluation of degradable electrospun polylactic acid/bioactive calcium phosphate ormoglass scaffoldscitations
- 2020Electrocatalytic Metallic Nanostructures Prepared By Electrorefining and Cathodic Corrosion
- 2019Effect of Pt Deposits on TiO2Electrocatalytic Activity Highlighted by Electron Tomographycitations
- 2017New synthesis route to decorate Li 4 Ti 5 O 12 grains with GO flakescitations
- 2016STEM study of Li4Ti5O12 anode material modified with Ag nanoparticlescitations
- 2016A novel hybrid nanofibrous strategy to target progenitor cells for a cost-effective in situ angiogenesiscitations
- 2014Anodic polarization of nanocrystalline titaniumcitations
Places of action
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article
STEM study of Li4Ti5O12 anode material modified with Ag nanoparticles
Abstract
Comprehensive scanning transmission electron microscopy(STEM) analysis of Li4Ti5O12 (LTO) powder modified by deposited Ag nanoparticles was performed. Nanocomposite powders with Ag content of 1 wt.%, 4 wt.%, 10 wt.% were fabricated in a chemical process from suspensions of Ag and LTO. Apart from the STEM results, the presence of pure silver on the surface of the ceramic powder was confirmed by XRD and XPS analyses. The silver particles deposited on the LTO particles were characterized using the EDS mapping technique. The quantified results of the EDS mapping showed a relatively homogenous distribution of silver nanoparticles on the powder surface for every metal content. The mean diameter of the nanoparticles deposited on the LTO powder was about 4 nm in all cases. An increase in the Ag content during chemical surfacemodification did not cause changes in themicrostructure. Focusing on an analysis of the metallic nanoparticles on the ceramic powder, electron tomography was used as an investigative technique. A very precise analysis of three dimensional nanostructures is desirable for a comprehensive analysis of complex materials. The quantified analysis of the Ag nanoparticles visualized using electron tomography confirmed the results of the size measurements taken from the two-dimensional EDS maps.