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Sukurov, Bolat M.
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article
Crystal Structure and Thermodynamic Properties of Barium–Thulium Bismuthate with Perovskite Structure
Abstract
<jats:p>A new sample of triple oxides—barium–thulium bismuthate <jats:styled-content style="fixed-case"><jats:roman>Ba</jats:roman></jats:styled-content><jats:sub>2</jats:sub><jats:styled-content style="fixed-case"><jats:roman>TmBiO</jats:roman></jats:styled-content><jats:sub>6</jats:sub> with perovskite structure—has been synthesized by ceramic technology. The unit cell parameters of the sample and the coefficients of thermal expansion have been determined by the method of <jats:styled-content style="fixed-case">X</jats:styled-content>‐ray analysis. Thermal properties of the sample have been studied by <jats:styled-content style="fixed-case">DTA</jats:styled-content> over the temperature range of 293–1473 K. The heat capacity of the compound has been measured over the range of 5–320 K by vacuum adiabatic calorimetry. Thermodynamic functions of the compound have been determined based on the heat capacity data.</jats:p>