| People | Locations | Statistics |
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| Naji, M. |
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| Motta, Antonella |
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| Aletan, Dirar |
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| Mohamed, Tarek |
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| Ertürk, Emre |
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| Taccardi, Nicola |
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| Kononenko, Denys |
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| Petrov, R. H. | Madrid |
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| Alshaaer, Mazen | Brussels |
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| Bih, L. |
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| Casati, R. |
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| Muller, Hermance |
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| Kočí, Jan | Prague |
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| Šuljagić, Marija |
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| Kalteremidou, Kalliopi-Artemi | Brussels |
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| Azam, Siraj |
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| Ospanova, Alyiya |
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| Blanpain, Bart |
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| Ali, M. A. |
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| Popa, V. |
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| Rančić, M. |
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| Ollier, Nadège |
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| Azevedo, Nuno Monteiro |
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| Landes, Michael |
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| Rignanese, Gian-Marco |
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Agersted, Karsten
Technical University of Denmark
in Cooperation with on an Cooperation-Score of 37%
Topics
Publications (29/29 displayed)
- 2019Influence of sintering profile on the microstructure and electronic transport properties of Sr(Ti,Nb)O3 tapes for solid oxide cell applications
- 2018Commercial alkaline earth boroaluminosilicate glasses for sealing solid oxide cell stacks. Part I: Development of glass-ceramic microstructure and thermomechanical propertiescitations
- 2018A Ba-free sealing glass with a high CTE and excellent interface stability optimized for SOFC/SOEC stack applicationscitations
- 2018A Ba-free sealing glass with a high CTE and excellent interface stability optimized for SOFC/SOEC stack applicationscitations
- 2018Commercial alkaline earth boroaluminosilicate glasses for sealing solid oxide cell stacks Part II: Characterization of devitrification and glass-ceramic phase assemblagescitations
- 2017Lattice constant measurement from electron backscatter diffraction patternscitations
- 2017Investigation of Cu 2 ZnSnS 4 nanoparticles for thin-film solar cell applicationscitations
- 2017A Novel SOFC/SOEC Sealing Glass with a Low SiO2 Content and a High Thermal Expansion Coefficient
- 2017Investigation of Cu2ZnSnS4 nanoparticles for thin-film solar cell applicationscitations
- 2017Mechanical properties of biaxially strained poly(L-lactide) tubes: Strain rate and temperature dependencecitations
- 2017A Novel SOFC/SOEC Sealing Glass with a Low SiO2 Content and a High Thermal Expansion Coefficientcitations
- 2017A Novel SOFC/SOEC Sealing Glass with a Low SiO 2 Content and a High Thermal Expansion Coefficientcitations
- 2016Characterization Of Biaxial Strain Of Poly(L-Lactide) Tubescitations
- 2015Ultrafast microwave hydrothermal synthesis and characterization of Bi1-xLaxFeO3 micronized particlescitations
- 2015Environmental TEM study of the dynamic nanoscaled morphology of NiO/YSZ during reductioncitations
- 2014NiO/YSZ Reduction for SOFC/SOEC Studied In Situ by Environmental Transmission Electron Microscopycitations
- 2014Fracture toughness of glass sealants for solid oxide fuel cell applicationcitations
- 2014Fabrication and sealing performance of rare-earth containing glass–ceramic seals for intermediate temperature solid oxide fuel cell applicationscitations
- 2014Effects of thermal aging on thermo-mechanical behavior of a glass sealant for solid oxide cell applicationscitations
- 2014Sintering and Electrical Characterization of La and Nb Co‐doped SrTiO3 Electrode Materials for Solid Oxide Cell Applicationscitations
- 2013Ion beam polishing for three-dimensional electron backscattered diffractioncitations
- 2013Two and three dimensional electron backscattered diffraction analysis of solid oxide cells materials
- 2013Bonding characteristics of glass seal/metallic interconnect for SOFC applications: Comparative study on chemical and mechanical properties of the interface
- 2013Bonding characteristics of glass seal/metallic interconnect for SOFC applications: Comparative study on chemical and mechanical properties of the interface
- 2012Effects of focused ion beam milling on electron backscatter diffraction patterns in strontium titanate and stabilized zirconiacitations
- 2012Microstructural and electrical characterization of Nb-doped SrTiO3–YSZ composites for solid oxide cell electrodescitations
- 2010A method of producing a multilayer barrier structure for a solid oxide fuel cell
- 2007Mechanical Behaviour of Glassy Composite Seals for IT-SOFC Applicationcitations
- 2006Testing of Ni-plated ferritic steel interconnect in SOFC stackscitations
Places of action
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article
Effects of focused ion beam milling on electron backscatter diffraction patterns in strontium titanate and stabilized zirconia
Abstract
This study investigates the effect of focused ion beam (FIB) current and accelerating voltage on electron backscatter diffraction pattern quality of yttria‐stabilized zirconia (YSZ) and Nb‐doped strontium titanate (STN) to optimize data quality and acquisition time for 3D‐EBSD experiments by FIB serial sectioning. Band contrast and band slope were used to describe the pattern quality. The FIB probe currents investigated ranged from 100 to 5000 pA and the accelerating voltage was either 30 or 5 kV. The results show that 30 kV FIB milling induced a significant reduction of the pattern quality of STN samples compared to a mechanically polished surface but yielded a high pattern quality on YSZ. The difference between STN and YSZ pattern quality is thought to be caused by difference in the degree of ion damage as their backscatter coefficients and ion penetration depths are virtually identical. Reducing the FIB probe current from 5000to 100 pA improved the pattern quality by 20% for STN but only showed a marginal improvement for YSZ. On STN, a conductive coating can help to improve the pattern quality and 5 kV polishing can lead to a 100% improvement of the pattern quality relatively to 30 kV FIB milling. For 3D‐EBSD experiments of a material such as STN, it is recommended to combine a high kV FIB milling and low kV polishing for each slice in order to optimize the data quality and acquisition time.