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Ammari, Lahcen El
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article
Crystal structure of barium dinickel(II) iron(III) tris[orthophosphate(V)], BaNi<sub>2</sub>Fe(PO<sub>4</sub>)<sub>3</sub>
Abstract
<jats:p>The orthophosphate BaNi<jats:sub>2</jats:sub>Fe(PO<jats:sub>4</jats:sub>)<jats:sub>3</jats:sub> has been synthesized by a solid-state reaction route and characterized by single-crystal X-ray diffraction and energy-dispersive X-ray spectroscopy. The crystal structure comprises (100) sheets made up of [Ni<jats:sub>2</jats:sub>O<jats:sub>10</jats:sub>] dimers that are linked to two PO<jats:sub>4</jats:sub> tetrahedra <jats:italic>via</jats:italic> common edges and vertices and of linear infinite [010] chains of corner-sharing [FeO<jats:sub>6</jats:sub>] octahedra and [PO<jats:sub>4</jats:sub>] tetrahedra. The linkage of the sheets and chains into a framework is accomplished through common vertices of PO<jats:sub>4</jats:sub> tetrahedra and [FeO<jats:sub>6</jats:sub>] octahedra. The framework is perforated by channels in which positionally disordered Ba<jats:sup>2+</jats:sup> cations are located.</jats:p>