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Naji, M. |
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Motta, Antonella |
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Aletan, Dirar |
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Mohamed, Tarek |
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Ertürk, Emre |
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Taccardi, Nicola |
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Kononenko, Denys |
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Petrov, R. H. | Madrid |
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Alshaaer, Mazen | Brussels |
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Bih, L. |
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Casati, R. |
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Muller, Hermance |
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Kočí, Jan | Prague |
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Šuljagić, Marija |
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Kalteremidou, Kalliopi-Artemi | Brussels |
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Azam, Siraj |
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Ospanova, Alyiya |
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Blanpain, Bart |
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Ali, M. A. |
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Popa, V. |
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Rančić, M. |
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Ollier, Nadège |
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Azevedo, Nuno Monteiro |
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Landes, Michael |
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Rignanese, Gian-Marco |
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Mugnaioli, Enrico
in Cooperation with on an Cooperation-Score of 37%
Topics
Publications (23/23 displayed)
- 2022Halide perovskites as disposable epitaxial templates for the phase-selective synthesis of lead sulfochloride nanocrystalscitations
- 2021Titania-decorated hybrid nano-architectures and their preliminary assessment in catalytic applications
- 2020Structural study of decrespignyite-(Y), a complex yttrium rare earth copper carbonate chloride, by three-dimensional electron and synchrotron powder diffraction
- 2020Nanocrystals of Lead Chalcohalides:A Series of Kinetically Trapped Metastable Nanostructurescitations
- 2020Nanocrystals of Lead Chalcohalidescitations
- 2020Cs 3 Cu 4 In 2 Cl 13 Nanocrystals:A Perovskite-Related Structure with Inorganic Clusters at A Sitescitations
- 2020Cs3Cu4In2Cl13 Nanocrystalscitations
- 20193D Electron Diffraction: The Nanocrystallography Revolutioncitations
- 2018Crystal Structures of Two Important Pharmaceuticals Solved by 3D Precession Electron Diffraction Tomographycitations
- 2018Ab initio structure determination of Cu2- xTe plasmonic nanocrystals by precession-assisted electron diffraction tomography and HAADF-STEM imagingcitations
- 2018Ab Initio Structure Determination of Cu2- xTe Plasmonic Nanocrystals by Precession-Assisted Electron Diffraction Tomography and HAADF-STEM Imagingcitations
- 2017Mineralogical, crystallographic and redox features of the earliest stages of fluid alteration in CM chondritescitations
- 2017The structure of denisovite, a fibrous nanocrystalline polytypic disordered 'very complex' silicate, studied by a synergistic multi-disciplinary approach employing methods of electron crystallography and X-ray powder diffractioncitations
- 2017The structure of denisovite, a fibrous nanocrystalline polytypic disordered 'very complex' silicate, studied by a synergistic multi-disciplinary approach employing methods of electron crystallography and X-ray powder diffractioncitations
- 2016Hierachical Ni@Fe2O3 superparticles through epitaxial growth of gamma-Fe2O3 nanorods on in situ formed Ni nanoplatescitations
- 2015Electron diffraction tomography for the characterization of sub-micrometric minerals: application to metamict phases
- 2015Structural insights into<i>M</i><sub>2</sub>O–Al<sub>2</sub>O<sub>3</sub>–WO<sub>3</sub>(<i>M</i>= Na, K) system by electron diffraction tomographycitations
- 2015Structural insights into M2O–Al2O3–WO3 (M = Na, K) system by electron diffraction tomographycitations
- 2015Single nano crystal analysis using automated electron diffraction tomographycitations
- 2014Rational assembly and dual functionalization of Au@MnO heteroparticles on TiO2 nanowirescitations
- 2014Atomic structure solution of the complex quasicrystal approximant Al77Rh15Ru8 from electron diffraction datacitations
- 2013A multi-technique characterisation of cronstedtite synthetized by iron-clay interaction in a step by step cooling procedurecitations
- 2009Electron diffraction, X-ray powder diffraction and pair-distribution-function analyses to determine the crystal structures of Pigment Yellow 213, C<sub>23</sub>H<sub>21</sub>N<sub>5</sub>O<sub>9</sub>citations
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article
Structural insights into<i>M</i><sub>2</sub>O–Al<sub>2</sub>O<sub>3</sub>–WO<sub>3</sub>(<i>M</i>= Na, K) system by electron diffraction tomography
Abstract
<jats:p>The<jats:italic>M</jats:italic><jats:sub>2</jats:sub>O–Al<jats:sub>2</jats:sub>O<jats:sub>3</jats:sub>–WO<jats:sub>3</jats:sub>(<jats:italic>M</jats:italic>= alkaline metals) system has attracted the attention of the scientific community because some of its members showed potential applications as single crystalline media for tunable solid-state lasers. These materials behave as promising laser host materials due to their high and continuous transparency in the wide range of the near-IR region. A systematic investigation of these phases is nonetheless hampered because it is impossible to produce large crystals and only in a few cases a pure synthetic product can be achieved. Despite substantial advances in X-ray powder diffraction methods, structure investigation on nanoscale is still challenging, especially when the sample is polycrystalline and the structures are affected by pseudo-symmetry. Electron diffraction has the advantage of collecting data from single nanoscopic crystals, but it is frequently limited by incompleteness and dynamical effects. Automated diffraction tomography (ADT) recently emerged as an alternative approach able to collect more complete three-dimensional electron diffraction data and at the same time to significantly reduce dynamical scattering. ADT data have been shown to be suitable for<jats:italic>ab</jats:italic><jats:italic>initio</jats:italic>structure solution of phases with large cell parameters, and for detecting pseudo-symmetry that was undetected in X-ray powder data. In this work we present the structure investigation of two hitherto undetermined compounds, K<jats:sub>5</jats:sub>Al(W<jats:sub>3</jats:sub>O<jats:sub>11</jats:sub>)<jats:sub>2</jats:sub>and NaAl(WO<jats:sub>4</jats:sub>)<jats:sub>2</jats:sub>, by a combination of electron diffraction tomography and precession electron diffraction. We also stress how electron diffraction tomography can be used to obtain direct information about symmetry and pseudo-symmetry for nanocrystalline phases, even when available only in polyphasic mixtures.</jats:p>